Page 42 - Application Notebook - Solution for Food Development

Application No.M271
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n Results
Samples of the three sake types were labeled as futsu-
shu, junmai-shu, and daiginjo-shu. Taking the results 2
from analysis, peak identification was performed based Futsu-shu

Futsu-shu 3
on the NIST 14 library and quantitative ions, reference 1 Daiginjo-shu
ions, and retention indices mentioned in previous Futsu-shu 2 Futsu-shu 1 Daiginjo-shu1
articles*. The numbers of compounds identified are t[2] 0
shown in Table 2. The 86 compounds detected by this Daiginjo-shu 2 Daiginjo-shu 3
analysis are also listed in Table 3. -1 Junmai-shu 1 Junmai-shu 3
Junmai-shu 2
Junmai-shu
-2
Table 2 Numbers of Compounds Detected
by Aroma Compound Analysis -3
-10 -8 -6 -4 -2 0 2 4 6 8
Futsu-shu Junmai-shu Daiginjo-shu t[1]
Detected 78 76 86
compounds Fig. 1 Score Plot of Aroma Compound Analysis

Principal Component Analysis (PCA) was performed for
the 76 compounds detected in all samples. A score plot Ethyl actate
of this analysis is shown in Fig. 1. The three different 0.6
sake types are clearly separated on the score plot. A Isobutanol
loading plot of this analysis is shown in Fig. 2. 0.4
Compounds characteristic to each sample were 3-methylbutyl acetate
identified from these results. t [2] 0.2 Pentyl acetate 3-methyl -
1-butanol
The results suggest that performing a complete analysis 0
of aroma compounds and subsequent multivariate 2-phenlyethanol
analysis of identified compounds may be useful for -0.2 1-butanol
food quality evaluation. 2-phenlyetyl acetate
-0.4 Furfural
-0.2 -0.1 0 0.1 0.2 0.3 0.4 0.5 0.6

Fig. 2 Loading Plot of Aroma Compound Analysis

Table 3 List of Compounds Detected by Aroma Compound Analysis (86 Compounds)
ethyl acetate 3-methylbutyl propanoate 2-ethyl-1-hexanol 1-decanol
3-methylbutanal 4-pentenyl acetate decanal β-citronellol
2, 4, 5-trimethyl-1,3-dioxolane 3-methyl-1-butanol 2-nonanol diethyl pentanedioate
ethyl propanoate ethyl hexanoate ethyl 3-hydroxybutanoate ethyl phenylacetate
ethyl 2-methylpropanoate 3-octanone benzaldehyde 2-phenylethyl acetate
propyl acetate styrene ethyl 2-hydroxyhexanoate 2- (2-butoxyethoxy) ethyl acetate
2, 3-butanedione hexyl acetate propanoic acid hexanoic acid
isobutyl acetate 2-octanone 1-octanol benzyl alcohol
ethyl butanoate octanal 3-methylbutyl methoxyacetate diethyl hexanedioate
1-propanol acetoin ethyl 3-methylthiopropanoate butylated hydroxytoluene
ethyl 2-methylbutanoate 2-heptanol ethyl decanoate 2-phenylethanol
ethyl 3-methylbutanoate 3-methyl-1-pentanol butyrolactone heptanoic acid
butyl acetate ethyl heptanoate 1-nonanol phenol
DMDS ethyl lactate acetophenone dehydromevalonic lactone
1- (1-ethoxyethoxy) pentane 1-hexanol phenylacetaldehyde octanoic acid
isobutanol 3-ethoxy-1-propanol furanmethanol ethyl hexadecanoate
3-methylbutyl acetate 2-nonanone ethyl benzoate decanoic acid
ethyl pentanoate ethyl octanoate diethyl succinate 2-phenylethyl octanoate
1-butanol 1-heptanol (Z)-3-nonen-1-ol benzoic acid
ethyl 2-butenoate 3-methylbutyl hexanoate 3-methylthio-1-propanol dodecanoic acid
pentyl acetate acetic acid pentanoic acid
2-heptanone furfural naphthalene