Page 44 - Application Notebook - PFAS Analysis
P. 44

No. SSI-LCMS-106



               ■ Summary and Conclusions
               The app note evaluated EPA SW-846 method 8327      Good linearity, accuracy, and precision for all PFAS
               for the direct injection analysis of 24 PFASs and 19   compounds included in draft EPA Method 8327
               mass-labeled surrogates in non-potable waters      were achieved. Hence, the Shimadzu LCMS-8050
               (namely ground water, surface water and            could achieve rapid, reliable and highly-sensitive

               wastewater) using Shimadzu UFMS™ LCMS-8050.        quantitative results in non-potable waters, allowing
               The data referenced in this article shows excellent   for high-throughput and fast turnaround times.
               performance of the LCMS-8050 for PFAS analysis in
               challenging environmental matrices with minimal
               sample preparation.

               ■ References
                   1.  Environmental Science and Technology. “Polyfluorinated Compounds: Past, Present, and Future”
                       http://www.greensciencepolicy.org/wp-content/uploads/2014/10/Lindstrom-Strynar-and-Libelo-2011.pdf

                   2.  Agency for toxic Substances and Disease Registry, “Per- and Polyfluoroalkyl Substances (PFAS) and Your
                       Health,” 31 October 2018. [Online]. Available:
                       https://www.atsdr.cdc.gov/pfas/. [Accessed 11 December 2018]

                   3.  U.S. Environmental Protection Agency (EPA). Per- and Polyfluoroalkyl Substances (PFAS)
                       https://www.epa.gov/pfas [Accessed November 27, 2018]

                   4.  National Institute of Environmental Health Sciences. Per- fluorinated Chemicals (PFCs)
                       https://www.niehs.nih.gov/health/matrials/perflorinated_chemicals_508.pdf [Accessed Nov 27, 2108]

                   5.  US EPA. Basic Information about Per- and Polyfluoroalkyl Substances (PFAS).
                       https://www.epa.gov/pfas/basic-information-about-and-polyfluoroalkyl-substances-pfass

                   6.  US EPA. Drinking Water Health Advisories for PFOA and PFOS. https://www.epa.gov/ground-water-and-
                       drinking-water/drinking-water-health-advisories-pfoa-and-pfos

                   7.  ASTM International, "ASTM D7979-17: Standard Test Method for Determination of Perfluorinated
                       Compounds in Water, Sludge, Influent, Effluent and Wastewater by Liquid Chromatography Tandem Mass
                       Spectrometry (LC/MS/MS)," West Conshohocken, 2017.

                   8.  ASTM D7979-17, Standard Test Method for Determination of Per- and Polyfluoroalkyl Substances in
                       Water, Sludge, Influent, Effluent and Wastewater by Liquid Chromatography Tandem Mass Spectrometry
                       (LC/MS/MS), ASTM International, West Conshohocken, PA, 2017, www.astm.org (Accessed November 27,
                       2018)

                   9.  Analysis of Per-and Polyfluoroalkyl Substances (PFAS) Specified in EPA M537.1 Using LCMS-8045. Brahm
                       Prakash, Gerard Byrne II, Ruth Marfil-Vega, Yuka Fujito, Christopher Gilles, Shimadzu Scientific
                       Instruments, Inc., Columbia, MD 21046
   39   40   41   42   43   44   45   46   47   48   49