Page 10 - Shimadzu SALD-7500nano

System Structure

Easy Measurement under PC Control Measurement Samples without Dilution
Sampler SALD-MS75 High-Concentration Measurement Unit: SALD-HC75

Groups of particles are dispersed in a liquid medium and measured High-concentration samples can be measured using the laser diffraction method.
as they are circulated between the flow cell, which is placed in the
measurement unit, and a dispersion bath in the sampler. Measurement is possible by simply holding the high-concentration sample particles to be measured between two glass slides.
The dispersion bath incorporates a stirrer and an ultrasonic sonicator. Samples for which the particle size distribution would be changed by dilution can be measured in their original state, or with the minimum required
A pump delivers the dispersed suspension to the flow cell. level of dilution, and a true image of the measurement object can be obtained.
The pump is specially designed to ensure both liquid medium and the Commercial hand creams, face creams, and rinses can be measured with hardly any pretreatment.
particles are circulated.
It can be controlled from a PC.
Flow Cell or Batch Cell Glass plates (Glass sides)
Most organic solvents can be used as dispersion media.
Solvent Resistance
Solvent Solvent Resistance Solvent Solvent Resistance Solvent Solvent Resistance Measurement unit Wing sensor II
Flow cell (Forward Scattered Light)
Acetone Applicable* note2 Xylene Applicable* note2 Isoplopyl Alcohol Applicable Side scattered Laser Light Diffracted/scattered light
light sensor Multiple Scattering
Isopropyl Alcohol Applicable Cyclohexane Applicable* note2 Hexane Applicable Laser Light
Ethyl Alcohol Applicable Cyclobenzene Applicable* note2 Benzene Applicable* note2
Laser light source
Ethylene Glycol Applicable Toluene Applicable* note2 Methyl Alcohol Applicable Backward scattered Condensing lens
light sensor Side /
length
Note1 Solvent resistance toward materials used in the passageways of SALD-MS75. Solvent resistance values are representative, and are not certified. back scattered light Light path
Note2 Only applicable for liquid pump. Not applicable for liquid supply pump. Dispersion Motor Optical Path Length
Note3 Ultrasonic cleaning instruments are needed for the measurement of reference sample.
medium
Measurement data Dispersion medium
supply pump
Q3(%) Q3(%) q3(%) If a standard flow cell or batch cell is used to measure a sample at high-concentration sample particles between two glass slides,
100 100 100 10
a high concentration, the long light pathlength results in multiple which shortens the length of the light paths, avoids the negative
Dispersion bath scattering, making it difficult to obtain accurate measurements. effects of multiple scattering and makes accurate measurement
8
80
80
Normalized Particle Amount (Cum) 60 40 60 40 Normalized Particle Amount (Cum) 60 40 6 4 Normalized Particle Amount (Diff) Circulation Drain valve With this system, however, it is possible to hold the possible.
80
pump
Ultrasonic sonicator
20
20
20
2
Sampler
0 0 500 0
0.01 0.05 0.1 0.5 1 5 10 50 100 500 0 0.01 0.05 0.1 0.5 1 5 10 50 100 Glass sample plates (glass with indentation) (Option)
Particle Diameter (µm) Particle Diameter (µm)
Drain
Variety of small and large sample particles Carbon nano tube Effective for measuring samples with relatively low concentrations, or expensive samples that can only be used in small amounts.
P/N Name Indentation depth Number Sample volume Particle concentration (% by weght) External Shape Round Indentation
Ideal for Measurement with Small Amounts of Organic Solvent 346-62295-01 Glass sample plate (0.1 mm) 0.1 mm (100 µm) 10 0.03 cm 3
346-62295-02 Glass sample plate (0.2 mm) 0.2 mm (200 µm) 10 0.06 cm 3
Batch Cell SALD-BC75 346-62295-03 Glass sample plate (0.3 mm) 0.3 mm (300 µm) 10 0.09 cm 3 A few hundred ppm
346-62295-04 Glass sample plate (0.4 mm) 0.4 mm (400 µm) 10 0.12 cm 3 to a few percent Indentation Depth
Measurement is possible with a small amount of sample (i.e., measured Cross
Funnel particles) and liquid medium (i.e., dispersion medium). 346-62295-05 Glass sample plate (0.5 mm) 0.5 mm (500 µm) 10 0.15 cm 3 Section
346-62295-06 Glass sample plate (0.05 mm) 0.05 mm (50 µm) 10 0.015 cm 3 (glass slide with indentation)
Glass Sample Plate
The capacity of the batch cell is only 5 cm so waste treatment for the 347-60002 Glass sample plate set 0.05 to 0.5 mm, two each 12 in total
3
suspension canbe performed with relatively small amounts. Application Example (depression cell)
Glass Slide
Laser beam Batch cell The vertical motions of the stirring plate prevent sedimentation of the particles. Glass Sample
Plate
The funnel reduces the possibility of sample spillage. Sample
Stroke of Measurement Data
vertical motion A tetrafluoroethylene resin funnel is provided to reduce the possibility
of suspension getting on the hands of the user. It also prevents the cell Q3(%) q3(%) Q3(%) q3(%)
100 20 100 20
surface from becoming dirty.
Measurement data Stirring plate
80 80
Q3(%) q3(%) Q3(%) q3(%) 15 15
100 100 100 20 60 60
80 80 80 Normalized Particle Amount (Cum) 10 Normalized Particle Amount (Diff) Normalized Particle Amount (Cum) 10 Normalized Particle Amount (Diff)
15 40 40
Normalized Particle Amount (Cum) 60 40 60 40 Normalized Particle Amount (Diff) Normalized Particle Amount (Cum) 60 40 10 Normalized Particle Amount (Diff) 20 5 20 5
20 20 20 5 0 0.01 0.05 0.1 0.5 1 Particle Diameter (µm) 5 10 50 100 500 0 0 0.01 0.05 0.1 0.5 1 Particle Diameter (µm) 5 10 50 100 500 0
Latex Wax
0 0 0 0
0.01 0.05 0.1 0.5 1 5 10 50 100 500 0.01 0.05 0.1 0.5 1 5 10 50 100 500
Particle Diameter (µm) Particle Diameter (µm)
Polystyrene Latex (20 nm, 30 nm, 50 nm) Silica particle
SALD-7500nano
10 Nano Particle Size Analyzer 11