Page 11 - Shimadzu MXF-2400
P. 11

11  Automatic Startup and Stop (Standby) of   14  Rapid and Precise Sample Setting
 Device is Possible

 The X-ray unit can be automatically started up by registering   The swing arm system sets a sample precisely within 5 seconds,
 the device startup date and time in advance.   in a single motion. This simple design minimizes down time and
 Automatic stop (standby) can be set in the same way.  ensures stable performance even in high-duty operation.


                            X-ray ON
                            40 kV
                            95 mA
                   Scanner 1
                   120.32 deg.
                   Scanner 2
                   90.23 deg.
                     Sample chamber
 Good Operability from Eight Sample
 12  Turrets with Dust-proof Cover  pressure  Turret
                     35 Pa
                     Device temperature
                     35˚C
 Standard samples and control samples can be safely set on the
                     Cooling water conductivity
 turrets for long periods as the device comes with   0.23 uS
 a dust proof cover.


            15    Automatic Qualitative Determination


            The scanning monochromator permits automatic qualitative
 Typical Detection Limits and Repeatability
            analysis.
            The 2θ-PHA linkage system (detector high voltage linkage
 13  High Sensitivity and High Precision  Low-alloy steel  Si  Mn  P  S  Ni  Integration time: 40 sec.  system) excludes the influence of higher-order lines to provide
 Cu
 Cr
            easy-to-read profiles.
 Mo
 Detection limit  0.0013  0.0006 0.00045 0.0004  0.0008  0.0002  0.0006 0.00045  In qualitative analysis, 8 samples many be continuously
 The adoption of the new X-ray tube of the end-window type   Concentration  0.223  0.66  0.015  0.017  1.99  0.69  0.042  0.19  analyzed, and then the peaks are identified and the results are
 and the short distance between the X-ray output port of the   Repeatability  Standard deviation   0.0011  0.0008 0.0002  0.00022 0.0016  0.0007  0.0003 0.00025  displayed and printed out.
 X-ray tube and the sample provides high intensity of the   Coefficient of variation 0.5  0.13  1.3  1.3  0.08  0.1  0.7  0.13
 fluorescent X-rays; this enhances the sensitivity for trace
 Cast iron  Integration time: 40 sec.
 elements and improves the detection limits.
 C  Si  Mn  P  S  Mg
 The use of curved crystals and curved dispersion elements
 Concentration  3.57  1.7  0.503  0.047  0.042  0.041
 enhances the resolution, while the adoption of a gas sealed
 Standard deviation  0.017 0.0017 0.0004 0.00025 0.0002 0.0008
 proportional counter, an automatic core wire winding type   Coefficient of variation  0.49  0.1  0.08  0.55  0.47  2
 detector, temperature control unit for the spectrometer, and the
 high-performance counting circuit provides high precision.  Copper alloy  Integration time: 40 sec.
 The degree of vacuum is controlled and stabilized by the CPU,   Cu  Zn  Mn  Si  Al  Sn  Pb  Fe
 which also enhances the stability of light-element analysis.  Concentration  57.0  38.0  0.26  0.014  0.06  0.17  0.011  0.019
 Standard deviation    0.01    0.01  0.00035 0.00068 0.00042 0.0007 0.00033 0.00027
 Coefficient of variation    0.018   0.026 0.13  4.8  0.7  0.4  3  1.4

 Ceramic cement  Integration time: 40 sec.
 SiO2  Al2O3  Fe2O3  CaO  MgO  SO3  Na2O  K2O
 Concentration  14.0  3.0  2.0  43.0  0.8  2.0  1.0  0.4
 Standard deviation    0.0063 0.0024 0.0008   0.006  0.004  0.0014  0.006  0.0005
 Coefficient of variation    0.045  0.08  0.04    0.014  0.5  0.07  0.6  0.13

                                                                                                  MXF-2400
 10                                                                                        Multi-Channel X-ray Fluorescence Spectrometer  11
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