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Small Spot Analysis Kit (Option)








            For Analysis of Small Contaminants and Defect Analysis in Small Regions
            This option can be used to analyze even smaller areas by replacing the collimator plate and sample
            observation camera. It is especially useful for analyzing trace foreign matter and defects in micro areas,
            and measuring plating thickness.

            Minimum 0.3 mm X-Ray Irradiation Diameter
            The excitation X-rays can be collimated to 0.3 mm in diameter, which is effective for the
            high-accuracy analysis of small contaminants and for defect analysis in small regions,
                                                                                        Sample Image at an Irradiation Diameter
            analyses difficult with standard specifications (minimum 1 mm in diameter).    of 0.3 mm (Extended Zoom)
                                                                                       Sample: stainless powder (approx. 0.1 mm)
            Enlarged Sample Images without Image Quality Degradation                        collected on filter paper
            This system supports smaller samples, which heightens the visibility of sample
            observation images. Users can switch to an enlarged image approximately 2.5 times
                                                                           Irradiation area
            larger than a previous image, without image quality degradation.  0.3 mm in diameter
                                                                           (yellow circle)
            Automatic Four-Stage Switching Between 0.3, 1, 3, and 10 mm in Diameter  Irradiation area
                                                                           1 mm in diameter
            The irradiation diameter automatically switches between 0.3, 1, 3, and 10 mm in diameter.   (green circle)
            This system supports not only the analysis of small spots but also macro composition
            analysis at 10 mm in diameter.
            Note: The irradiation diameter is the size on the sample surface.               Metal Plated Terminals
                                                                                      (At 1 mm in diameter, the irradiation area is not
            Irradiation diameter              Extended zoom button                    within the measurement area, so measurements
            switching buttons                 (Enlargement to approx.
                                               2.5 times the camera image)              are impossible. At 0.3 mm in diameter,
                                                                                           measurements are possible.)
                     PCEDX Navi Sample Image Setting Fields

            Analysis Example—Small Metal Powder (Approx. 0.1 mm in Diameter) Adhered to the Surface of Snacks
            A small metal powder approximately 0.1 mm in diameter adhered to the commercially available snacks was analyzed with irradiation diameters
            of 1 mm and 0.3 mm, respectively. At an irradiation diameter of 1 mm, the overall background is significantly increased due to the influence of
            scattered X-rays from the surrounding area of the metal powder (snacks), resulting in a poor S/N ratio. At an irradiation diameter of 0.3 mm,
            however, the influence of scattered X-rays from the surrounding area is small, and peak profiles with a good S/N ratio are obtained.
            Copper (Cu) and Zinc (Zn) are detected as the major components with both irradiation diameters. It indicates that the metal powder is brass
            regardless of the irradiation diameter used. However, at 0.3 mm in diameter, the peak of Lead (Pb) is also identified, which suggests that the
            metal powder is “free cutting brass”.
            By using an irradiation diameter of 0.3 mm, more accurate analyses can be performed, even for small contaminants on substances such as
            organic materials that strongly scatter X-rays.

                                                  CuKa     1mmø
                                                           0.3mmø          RhKaC
                                       CaKa
                                                   ZnKa
                                                           ZnKb
                                                                                Sample Image
                                                                            (The yellow circle at the center is 0.3 mm.)
                                                            PbLa  PbLb1
                                                    CuKb                      RhKa
                                        CaKb  FeKa   ZnKb       SrKa             RhKbC
                                      KKa               PbLa  PbLb1                 RhKb




                                                                                                                                                                                                                             EDX-7200
      26                                                                                                                                                                                                            Energy Dispersive X-Ray Fluorescence Spectrometer
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