Page 189 - Shimadu Consumables Catalog
P. 189

Capillary Columns
           PLOT Columns


              SH-Silica BOND
              Bonded silica stationary phase minimizes impact of water, resulting in reproducible retention times for water-containing samples.
              Versatile column ideal for analysis of light hydrocarbons, sulfur gases, halocarbons, and carbon dioxide.

              Individually QC tested with sensitive C4 probes to ensure consistent selectivity.
              Proprietary manufacturing process practically eliminates particle release, reducing downtime due to obstructed FID jets.
              Similar phases: GS-GASPRO, CP-SilicaPLOT


               ID                Temp. Range                                    30 m
             0.32 mm             -80 to 260 °C                                227-36620-02


           Sulfur Compounds in Propane



                     Peaks
                   1.   Carbonyl sulfide
                   2.   Propane                                                Conditions
                   3.   Hydrogen sulfide                                       Column       :  SH-Silica BOND,
                   4.   Carbon disulfide
                   5.   Methyl mercaptan                 4                                   30 m, 0.32 mm ID
                                                                                             (P/N: 227-36620-02)
                                                                              Sample Conc   :  6 ppm in 100% propane
                                                                              Inj.         :  Sample valve, split
                                                                                             (split flow: 40 mL/min)
                                                                              Sample Loop Vol.  :  250 μL
                                                                              Inj. Temp    :  250 °C
                                                                              Oven Temp    :  35 °C (hold 8 min) to
                                                                                             200 °C at 10 °C/min
                                                                                             (hold 5 min)
                                                                              Carrier Gas   :  He, constant flow rate
                                                                                             2 mL/min
                                                                              Detector     :  PFPD, 250 °C
                                                                  5           Element Mode   :  sulfur
                                                                              Acknowledgement :  Chromatogram courtesy
                                                                                             of Brix and Joeri Vercammen
                                                                                             (Global Analyser Solutions,
                                                                                             Belgium)
                                1




                                       3

                                   2



                           5.0          10.0         15.0          20.0          25.0
                                                    Time (min)






                                Trap columns for adhering dislodged particles from PLOT columns are also available.
                                                                                       Please refer to page C-45.








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