Page 184 - Shimadu Consumables Catalog
P. 184

GC Columns



           Capillary Columns
           Dedicated Columns


              SH-BAC Plus 1 / SH-BAC Plus 2
              Optimized column selectivities guarantee resolution of ethanol, internal standards, and frequently encountered interferences.

              Robust and reproducible column chemistry ensures longer column lifetime and consistent results.


           SH-BAC Plus 1
               ID       df         Temp. Range                                30 m
            0.32 mm   1.80 µm     -20 to 240/260 °C                        227-36260-01
            0.53 mm   3.00 µm     -20 to 240/260 °C                        227-36261-01

           SH-BAC Plus 2
               ID       df         Temp. Range                                30 m
            0.32 mm   0.60 µm     -20 to 240/260 °C                        227-36263-01
            0.53 mm   1.00 µm     -20 to 240/260 °C                        227-36264-01

           Analysis of Alcohol Compounds in Blood






                                                        SH-BAC Plus 2      Conditions
                                                                         Instrument   :  GC-2010 Plus AF + HS-20
                                                         Peaks           Headspace  :  Oven Temp.: 85 °C
                                                        1.  Acetaldehyde             Vial Warming Time: 15 min
                                                        2.  Methanol                 Vial Pressurization Time: 1 min
                                                        3.  Ethanol                  Injection Time: 0.5 min
                                                        4.  Acetone                  Sample Line Temp: 150 °C
                                                        5.  Isopropanol
                                                        6.  t-Butanol                Vial Volume: 20 mL
                                                        7.  1-Propanol               Vial Agitation: Off
                                                                                     Vial Pressurization: 100 kPa
                                                                                     Load Time: 0.5 min
                                                                                     Needle Flash Time: 0.5 min
                                                                                     Transfer Line Temp: 150 °C
                                                                         Column    :  SH-BAC Plus 2, 30 m, 0.32 mm ID,
                                                                                     0.60 μm (P/N: 227-36263-01)
                                                        SH-BAC Plus 1                SH-BAC Plus 1, 30 m, 0.32 mm ID,
                                                                                     1.80 μm (P/N: 227-36260-01)
                                                         Peaks           Column Temp  :  40 °C
                                                        1.  Acetaldehyde  Inj.     :  Split (split ratio: 20:1)
                                                        2.  Methanol     Carrier Gas   :  He, 100 kPa
                                                        3.  Ethanol      Detector  :  FID, 250 °C
                                                        4.  Acetone      Makeup Gas   :  He, 30 mL/min
                                                        5.  Isopropanol
                                                        6.  t-Butanol    Hydrogen  :  40 mL/min
                                                        7.  1-Propanol   Air       :  400 mL/min






















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