Page 181 - Shimadu Consumables Catalog

SH-CLP / SH-CLP II

Dedicated columns for organochlorine pesticides and herbicides.
Low bleed - ideal for high-sensitivity GC-ECD or GCMS analyses.
Baseline separations in less than 10 minutes.

Analyze EPA Method 8081B, 8082A, 8151A, 504.1, 515, 508.1, and 552.2 compounds without time-consuming column changes.
Similar phases: DB-CLP1 / DB-CLP2

SH-CLP

ID df Temp. Range 30 m
0.32 µm -20 to 320/340 °C 227-36266-01
0.32 mm
0.50 µm -20 to 320/340 °C 221-75879-30

SH-CLP II
ID df Temp. Range 30 m
0.32 mm 0.25 µm -20 to 320/340 °C 227-36267-01

Organochlorine Pesticides (US EPA Method 8081)

Peaks
1. 2,4,5,6-tetrachloro-m-xylene
2. α-BHC (α-HCH)
3. γ-BHC (lindane)
4. β-BHC (β-HCH)
5. δ-BHC (δ-HCH)
6. heptachlor
7. aldrin
8. heptachlor epoxide
9. γ-chlordane
10. α-chlordane
11. 4,4'-DDE
12. endosulfan I
13. dieldrin
14. endrin
15. 4,4'-DDD
16. endosulfan II
17. 4,4'-DDT
18. endrin aldehyde
19. methoxychlor
20. endosulfan sulfate
21. endrin ketone
22. decachlorobiphenyl

Conditions
Column : SH-CLP, 30 m, 0.32 mm ID, 0.50 μm SH-CLP2, 30 m, 0.32 mm ID, 0.25 μm
(P/N: 221-75879-30) (P/N: 227-36267-01)
Oven Temp : 120 °C (hold 1 min) to 300 °C (hold 10 min)
at 9 °C/min
Inj. : Direct
Inj. Temp : 200 °C
Detector : ECD, 300 °C with anode purge
Dead time : 1.9 min
Head pressure : 8.7 psi (constant)
Flow rate : 1.3 mL/min at 120 °C, He

Pg C-31