Page 162 - Shimadu Consumables Catalog
P. 162
GC Columns
SH-I-17Sil MS
Mid-polarity Crossbond™ phase (similar to 50% phenyl methyl polysiloxane) SH-I-17Sil MS Structure
Low bleed for use with sensitive detectors, such as MS.
$) $) $)
Excellent inertness and selectivity for active environmental compounds, such as PAHs. 4J 0 4J 3 4J 0 4J 0
Equivalent to USP G3 phase. $) $) $)
Y Z [
Similar phases: DB-17ms, HP-17, DB-17, VF-17ms, CP-Sil 24 CB
ID df Temp. Range 30 m 60 m
0.25 mm 0.25 µm 40 to 340/360 °C 221-75916-30 227-36071-01
0.32 mm 0.25 µm 40 to 340/360 °C 227-36072-01 −
* Maximum temperatures listed are for shorter length columns. Longer columns may have a different maximum temperature.
SH-I-PAH
Mid-polarity proprietary phase
Ideal for EFSA PAH4 analysis—separates all priority compounds: benz[a]anthracene, chrysene, benzo[b]fluoranthene and benzo[a]
pyrene.
Best resolution of chrysene from interfering PAHs, triphenylene, and cyclopenta[cd]pyrene.
Complete separation of benzo [b], [k], [j], and [a] fluoranthenes.
ID df Temp. Range 30 m 40 m 60 m
0.18 mm 0.07 µm to 360 °C − 227-36073-01 −
0.25 mm 0.10 µm to 360 °C 227-36074-01 − 227-36074-02
Polycyclic Aromatic Hydrocarbons (US EPA Method 8100)
Peaks 25. Dibenzo[a,e]pyrene
1. Naphthalene 26. Dibenzo(a,i)pyrene
2. 2-Methylnaphthalene 27. Dibenzo(a,h)pyrene
3. 1-Methylnaphthalene
4. Acenaphthylene
5. Acenaphthene
6. Fluorene
7. Phenanthrene
8. Anthracene
9. Fluoranthene
10. Pyrene
11. Benz[a]anthracene
12. Chrysene
13. Triphenylene
14. Benzo[b]fl uoranthene
15. Benzo[k]fl uoranthene
16. Benzo(j)fl uoranthene
17. Benzo[a]pyrene
18. 3-Methylcholanthrene
19. Dibenz(a,h)acridine
20. Dibenz[a,j]acridine
21. Indeno[1,2,3-cd]pyrene
22. Dibenz[a,h]anthracene
23. Benzo[ghi]perylene
24. 7H-Dibenzo[c,g]carbazole
Conditions
Column : SH-I-17Sil MS, 30 m, 0.25 mm ID, 0.25 um Oven Temp : 65 °C (hold 0.5 min) to 220 °C at 15 °C/min to 330 °C
(P/N: 221-75916-30) at 4 °C/min (hold 15 min)
Inj. Vol. : 0.5 μL splitless (hold 1.75 min) Carrier Gas : He, constant flow rate 2.0 mL/min
Inj. Temp : 320 °C Detector : FID, 320 °C
Purge Flow : 75 mL/min
Pg C-12
