Page 167 - Shimadu Consumables Catalog

Capillary Columns
General-Purpose Columns

SH-5MS
Low-polarity phase: Crossbond™ 5% diphenyl / 95% dimethyl polysiloxane SH-5MS Structure

Column specifically tested for low-bleed performance. $)

General-purpose columns for drugs, solvent impurities, pesticides, hydrocarbons, PCB 4J 0 4J 0
congeners (e.g., Aroclor mixes), essential oils, semi-volatiles.
$)
Equivalent to USP G27 and G36 phases.

Similar phases: HP-5, DB-5, CP-Sil 8 CB, SPB-5

For SH-I-5MS columns with Integra-Guard™ column, please refer to page C-44.

ID df Temp. Range 15 m 30 m 60 m
0.10 µm -60 to 330/350 °C 221-75854-15 221-75854-30 227-36122-01
0.25 µm -60 to 330/350 °C 221-75855-15 221-75855-30 227-36123-01
0.25 mm
0.50 µm -60 to 330/350 °C − 227-36124-01 227-36124-02
1.00 µm -60 to 325/350 °C − 221-75857-30 −
0.10 µm -60 to 330/350 °C − 227-36125-01 227-36125-02
0.25 µm -60 to 330/350 °C − 221-75858-30 221-75858-60
0.32 mm
0.50 µm -60 to 330/350 °C − 227-36126-01 227-36126-02
1.00 µm -60 to 325/350 °C − 227-36127-01 −
0.50 µm -60 to 320/340 °C − 221-76191-30 −
0.53 mm 1.00 µm -60 to 320/340 °C − 227-36128-01 −
1.50 µm -60 to 310/330 °C − 227-36129-01 −
* Maximum temperatures listed are for shorter length columns. Longer columns may have a different maximum temperature.

Endocrine Disruptors: Alkyl Phenols

Peaks
1. tert-butyl phenol
2. n-pentyl phenol
3. n-hexyl phenol
4. n-heptyl phenol
5. tert-octyl phenol
6. n-octyl phenol
7. n-nonyl phenol
8. bisphenol A

Conditions
Column : SH-5MS, 30 m, 0.25 mm ID, 0.25 μm (P/N: 221-75855-30).
Conc. : 5–10 ng on-column
Inj. : Splitless, purge on at 1 min
Inj. Temp : 275 °C
Purge Flow : 32.2 mL/min (20:1 split)
Oven Temp : 35 °C (hold 1 min) to 300 °C at 10 °C/min (hold 15 min)
Carrier Gas : He
Det. Temp : 310 °C

Pg C-17