Page 12 - Solutions for Plastic Evaluation
P. 12

Evaluation of Raw Materials
                             Additives
           LCMS-IT-TOF



    Evaluation of   Plastic Materials  Analysis of Additives in Polymer Extract Using LCMS-IT-TOF (Part 1)


                                                                                 An organic solvent (in this case, THF/
                                                                                 MeOH = 1/1) was added to a known
                                                                                 quantity of polymer beads. The samples
                                                                                 were then sonicated and the supernatant
                                                                                 was extracted and directly analyzed by
                                                                                 an LCMS-IT-TOF system. Measurement
    Evaluation of   Raw Materials                                                on the left.
                                                                                 results are shown in the chromatograms

                                                                                 Of  the  six  types  of  additive  peaks
                                                                                 observed, the below structural prediction
                                                                                 was performed for peak B.

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                         Example: Predicting the Structure for Peak B  Example: Analysis Using Formula Predictor




























                                                                    n
               The smaller the m/z number, the fewer the number of candidates. Using MS  analysis allowed the structural predictions to be narrowed
               down.




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