Page 40 - Solutions for Plastic Evaluation
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        Product Information
                             Liquid Chromatograph Mass Spectrometer
     Evaluation of Plastic Materials



    Evaluation of   Plastic Materials  Analysis of Polymer Additives Using LCMS
               The various types of additives added to polymer materials and products serve an important function that can determine that
               product's performance. For example, for the same type of polymer, the formulation of additives can vary depending on the
               brand or grade. This means that the information obtained from analyzing additives can be very important for market research or
               product development.

               Features of Shimadzu LCMS-2020
               Liquid Chromatograph Mass Spectrometers
    Evaluation of   Raw Materials  ▪ From HPLC to UFLC

                 In addition to speed and separation capabilities, ultra fast LC (UFLC) succeeds in
                 offering both higher precision and expandability than possible with conventional
                 high-performance LC (HPLC) systems.
               ▪ Ultra Fast Speed
                 To achieve overall faster processing speeds, the LCMS-2020 offers not only faster
     Product Evaluation  ▪ Exceptional Reproducibility                                      LCMS-2020
                 analysis, but also faster sample injection speeds and fully automated analytical
                 functions.


                 Even  though  the  LCMS-2020  is  ultra  fast  LC,  it  provides  very  high  injection
                 reproducibility. It also offers unrivaled carryover suppression, which is critical for
                 LC/MS analysis.
     Product Information  Using these features allows easily confirming the elution of components based on the
               ▪ Extensive Expandability
                 In addition to ultra-fast analysis, the system also offers the flexibility to be used
                 for many other applications as well, such as normal HPLC or semi-preparative LC.


               m/z value of known additives, highly selectively quantitating components, predicting
               the molecular weights of unknown compounds, and more.                LCMSsolution Ver. 5 for LCMS-2020

                Ultra-fast                      Ultra-fast                      Ultra-fast
                UFswitching                     UFsensitivity                   UFscanning
                Rapid 15-millisecond positive/negative   Superior sensitivity from UFLC  15,000 u/sec fast scanning speed
                ionization switching            The newly developed Qarray ®  Optics achieves superior   Controls the voltage applied to the Quadrupole
                                                sensitivity, reproducibility, and linearity.   according to the scan speed and m/z.
                To detect both positive and negative ions, analysis is
                                                                                This new technology (patent pending) maintains
                performed while switching between the positive and
                negative ionization modes.                                      resolution and achieves high ion transmittance even at
                                                                                high scanning speeds.
                The LCMS-2020 adopts a high-voltage power supply
                featuring novel technology (patent pending) to achieve
                an ultra-fast polarity switching time of just 15 ms.
                    Polarity switching time   Polarity switching time
                      15 msec  15 msec
                 Positive-ion   Negative-ion   Positive-ion
                 measurement   measurement   measurement
                 SIM 2CH  SIM 2CH  SIM 2CH




                                                                                                   m/z 414: L-α-Narcotine
                                                                                                   m/z  414: L-
                                                                                                   m/z
                                                                                                   m/z  256: Diphenhydramine
                                                                                                   m/z 256: Diphenhydramine
                                                                                                   m/z
                                                                                                   m/z  267: Desipramine
                                                                                                   m/z
                                                                                                   m/z 267: Desipramine
                                                                                                     278: Amitriptyline
                                                                                                   m/z 278: Amitriptyline
                                                                                                   m/z
                                                                                                   m/z
                                 Sample:
                                 m/z 321: Chloramphenicol
                                 m/z 344: Dibucaine
                                 m/z 329: Furosemide
                                 m/z 231: Isopropylantipyline
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