Page 61 - Application Handbook - TOC
P. 61

Sum parameter – Total Organic Carbon

                                         Kit for small sample volumes


                    SCA-130-505


            The instruments of the TOC-L  series are            ■ Small sample volumes
            designed to successively analyze many               It can also occur, however, that only a few mL
            different types of samples of different             of sample  are available. This is usually the
            concentrations. For the autosampler, sample         case when there is only little sample
            trays for  different sample numbers and             available, the sampling process is complex or
            sample volumes are available.                       the sample is very valuable. For such cases,
                                                                the kit for small sample volumes is available.
                                                                The 5 mL syringe body can be exchanged for
                                                                a 500 µL syringe in a rapid conversion step.
                                                                Moreover, the injection slider has to be
                                                                exchanged too.

                                                                ■ Specification
                                                                With    this  option,   automatic    dilution,
                                                                acidification and sparging is not possible and
                                                                the specifications are, therefore, changed as
                                                                follows:

                                                                Measurement range:  TC, IC: to 2,000 mg/L
                                                                                      TN: to 200 mg/L
                                                                Injection volume:    150µl maximal
                                                                Diameter:            0.2 mm
            To eliminate cross-contamination between            NPOC-Measurement:  In ASI-L with external
            analyses of the different samples, the number                            Sparge kit
            of rinsing  steps can be defined in the             ASI-L:               9ml Rack
            software. There is usually enough sample
            volume available to rinse the tubing and the        ■ Example
            injection system of the TOC-L several times.        5 mL sample is sufficient for NPOC
            Depending on the measuring method,                  determination using an ASI-L, 9mL vials
            injection volume, measurement range and             (3 injections with 150 µL injection volumes)
            rinsing steps, 10 – 20  mL of the  sample is
            needed.
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