Page 33 - Shimadzu Journal vol.8 Issue2
P. 33

Latest topics 1

                 Introducing Refinery Gas Analyzer


                          with trace Sulfur detection






            Refinery gas is produced during crude oil refining. Typical com-  Shimadzu recently launched highly sensitive Nexis SCD-2030
            position is C1-C5 Paraffins, C6+ Paraffins, C2-C5 Olefins and   used  in  well-established  High-Speed  Refinery  Gas  Analyzer  for
            non-condensable gases like H2, O2, N2, CO and CO2. This gas   speciation  and  quantification  of  trace  sulfur components.  This
            is also used as petrochemical feed stock that is used in several   complete system, which uses 4 detectors simultaneously, is very
            catalytic processes. Determining the composition of Refinery gas   accurate and robust.
            and measurement of trace sulfur content is very important. Trace
            amount of sulfurs can poison the catalyst used in processes, which   This system is in compliance with ASTM D7833, D5504, D5623,
            can cost millions of dollars.                      D1945, D1946, D2163, UOP 539.


                                                               Following are the main features of the system
                                                                 — Robust system uses 2 TCD, 1 FID and SCD detector
                                                                 —  Simultaneous analysis of Hydrocarbons and Sulfur can be performed
                                                                 —  Highest sensitivity and very low maintenance Nexis SCD-2030
                                                                 — Faster analysis time


                                                               For this analysis, process gas stream having all above components
                                                               is injected into the system based on Shimadzu Nexis GC- 2030
                                                               with 4 detectors - 2 TCDs, FID and SCD. Four sample loops are
                                                               filled with sample and injected onto the columns. Respective col-
                                                               umns do the separation of required components which are then
                                                               analyzed by the respective detectors.

                                                               Shimadzu uses parallel valve configuration with backflush for light
                                                               gases and light hydrocarbons. This way system becomes very
                                                               simple and can be maintained easily.






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