Page 17 - Shimadzu MXF-2400
P. 17

7  X-R Administration Diagram  8  Automatic Operation System  11  Qualitative Analysis  13  Four Types of Matching Functions
 (α-β Administration Diagram)
 Unmanned operation is possible through the use of   The scanner is used to perform qualitative analysis and the   1) Impurity Judgment
 The change in analytical values over time can be displayed   functions such as a timer to automatically start up the system   profiles will be displayed and can be printed out.  Compares the unknown sample with standard sample
 graphically to enable observation of whether or not analysis   and halt it (put it on standby) after analysis is completed.  Also, analysis result reports can be created with profile   values to judge whether or not it belongs to the same
 values have stably entered the specified range.  images if the data is combined with a tool like Word Pad.  form.
                                                                  2) Product Type Classification
                                                                    Registers element standard values and tolerance of
                                                                    multiple forms to judge what form the unknown
                                                                    sample is.
                                                                  3) Form Judgment
                                                                    Registers the element content range for multiple forms
                                                                    to judge what form the unknown sample is.
                                                                  4) Matching Search
                                                                    Registers the standard values for multiple forms and
                                                                    searches for a match with the least differences
                                                                    between unknown sample and standard values.







 9  Calibration Curve  10  Matrix Correction  12  Quantitative Analysis Possible using
               FP Method
 The optimal calibration curve coefficient is calculated by   For samples with multiple elements, different measuring
               Quantitative analysis is possible with the FP method –
 the method of least squares using the standard sample.  X-ray intensities will occur depending on the composition
               which does not need a standard sample – using the
 W = aI 2  + bI + c  ratio of the main components, which may cause analysis
               scanner and fixed beam monochromators.
 W       : Element concentration  errors. Analysis precision is enhanced if matrix correction is
 I          : X-ray intensity  used.
 a, b, c : Calibration constants
 As well as being displayed in graph form, the calibration
 curve shows the calibration constants, precision and
 correlation coefficient, etc.
 Graph display size also can be freely expanded and
 reduced.

























                                                                                                  MXF-2400
 16                                                                                        Multi-Channel X-ray Fluorescence Spectrometer  17
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