Page 6 - Shimadzu ICPMS-2030 Series
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Two Assistant Functions Simplify Analysis






                     The Development Assistant simpli es the process of developing analytical methods. The Diagnosis Assistant automat-
                     ically diagnoses spectral interference. Together, they provide analytical results with exceptionally high reliability.

                     Development Assistant Function Ensures Analytical

                     Methods Can Be Developed with Con dence by Anyone.


                       Development Assistant

                     Creating analytical methods for ICPMS-2030 Series analysis involves only selecting the measured and target elements, even for
                     samples being analyzed for the  rst time. Then, based on the qualitative analysis data (for all mass numbers) from a represen-
                     tative sample, the Development Assistant automatically selects the optimal mass numbers and internal standard elements for
                     the target measurement elements and automatically speci es the concentration range for calibration curve samples.


                      Conventional Method Development Process           Creating Analytical Method Using
                        (when analyzing a sample for the  rst time)          Development Assistant




                           Prepare sample (pretreat sample)              Prepare sample (pretreat sample)



                          Qualitatively analyze all elements            Qualitatively analyze all elements



                         Determine optimal mass numbers for            Select target measurement elements
                            target measurement elements
                                                                        The Development Assistant function automatically sets the
                                                                        optimal mass numbers and internal standard elements for the
                          (1) Isobaric ions
                          (2) Oxide ions (Check mass numbers 16 less than target mass numbers.)  target measurement elements, and suggests a calibration
                          (3) Divalent ions (Check mass numbers twice the target mass numbers.)  scheme.
                          Example: Determining optimal mass number for Cd
                          (1) Select mass number from mass number list.                                 2 min
                               → Select 111 Cd with no isobaric ions.  Method completed in 2 minutes
                          (2) Check spectra for oxide ions (111 − 16 = 95) that might
                               interfere with 111 Cd.
                          (3) Check spectra for divalent ions ((111 × 2) = 222).

                               Select internal standards
                       (Select optimal elements and mass numbers)
                          Criteria for selecting internal standard elements
                          1. Quantity in sample is less than 1/100 of quantity added.
                          2. Mass number is near target measurement element.
                          3. Ionization energy is close to ionization energy of measurement element.
                          4. Not easily affected by spectral interference
                          5. Does not cause interference with spectra of target measurement elements.
                          6. Elements and mass numbers are detectable with suf cient sensitivity.

                           Specify calibration curve sample




                                                          10 min
                       Method completed in 10 minutes



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