Page 5 - Shimadzu DTG-60 Series

Simultaneous TG/DTA DTG

DTG-60 Series

Simultaneous TG/DTA improves ease of operation, High sample throughput Fully controlled atmosphere for various applications
sensitivity and analytical accuracy of conventional The built-in cooling fan and the low-mass furnace allow very ef cient cooling During TG/DTA measurements, qualitative and quantitative analysis, examination
standalone systems. times. After the completion of the measurement, the cooling starts of reaction mechanisms and evaluation of heat resistance are performed by
studying various reactions and interactions between a sample and special
automatically and stops when the furnace has reached a preset temperature.
Now the next analysis can be started. Cyclic and cooling runs are under full atmospheres. The unique channel structure of the DTG-60 series offers the
If exibility and high performance is needed in various applications, the new instrument control. solution for these applications. While an inert gas purges the balance, reactive
DTG-60/60H combines them all: Basic functions required by simultaneous gases are directly connected to the reaction pan.
thermogravimetry/differential thermal analysis (TG/DTA) measurements are improved.
Atmosphere control is programmable. As in DSC, the TA-60WS provides advanced Gas Out Cleaning Gas In
acquisition, analysis and report functions which ensure comfortable simultaneous
Gas In
measurements.

High sensitivity and high precision of balance is Solenoid
Valve
equivalent to dedicated single-function instruments
Model DTG-60 series has a unique balance mechanism (Roberval mechanism) that The change in the center
prevents changes in sensitivity from factors such as thermal expansion and allows high of gravity does not matter. Setting for the Cooling fan control parameter (Detector properties box) Gas In
precision thermogravimetric measurements. Furthermore, the fulcrum used for the Vacuum Pump
balance is made from thin alloy metal strips that have tiny thermal coefficients and are
crossed to form an "x" shape. This fulcrum (X-shaped fulcrum) is lightweight and has
extremely low friction and resistance. Using this fulcrum configuration allows The load is applied at
incorporating a highly sensitive balance and is even highly resistant to vibration. the same point no matter
where the sample is placed. DTG-60A/60AH provides a High sensitivity DTA detectors
compact built-in autosampler
Up to 24 samples can be setup for analysis. In addition, the weight of empty
TGA DTA
mg µV cell and sample can be measured automatically.
TG −12.353%
0.0
−19.020%
100.0
−30.196%
−0.5
DTA 0.0
−1.0
679.05˚C X-Shaped Fulcrum
164.75˚C
200.0 400.0 600.0 800.0
Temp [˚C]

Measurement of trace CaC2O4
Furnace
Specifications
TGA DTA Sample
mg µV Holder DTG-60 DTG-60H DTG-60A DTG-60AH
Rubber Balance principle Parallel guide differential top pan type
0.0 TG Substances 2000 Temperature range Ambient to 1100℃ Ambient to 1500℃ Ambient to 1100℃ Ambient to 1500℃
−68.281%
−10.0 Carbon Black Furnace Base Measurable range (TG) ±500mg
−28.158% Measurable range (DTA) ±1000µV
↑ 1000 Beam
−20.0 Switches from Joint Section Weight readability 0.1µg
nitrogen to air Shutter Sample quantity 1g Max. in gross weight
−30.0 Coil Atmosphere Air and inert gas
DTA 0 Auto sampler ─ 24 samples / tray
−40.0 Magnet Standard sample ─ Fixed
0.0 200.0 400.0 600.0 800.0 X-Shaped Fulcrum Analysis / Print ─ Automatic analysis and automatic report printout
Temp [˚C] Photoelectric Size W 367×D 650×H 453mm
Conversion Element
Measurement of carbon black in SBR Lamp Weight 35kg 40kg
AC 100 V, 120 V, 230 V, AC 100 V, 120 V, 230 V, AC 100 V, 120 V, 230 V, AC 100 V, 120 V, 230 V,
Power supplySpecifications
1300 VA, 50/60 Hz 1500 VA, 50/60 Hz 1300 VA, 50/60 Hz 1500 VA, 50/60 Hz

60 Series
4 Thermal Analysis Instruments 5