Page 4 - Shimadzu DTG-60 Series
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Simultaneous TG/DTA        DTG


                                            DTG-60 Series


                                            Simultaneous TG/DTA improves ease of operation,                                           High sample throughput                             Fully controlled atmosphere for various applications
                                            sensitivity and analytical accuracy of conventional                                       The built-in cooling fan and the low-mass furnace allow very ef cient cooling   During TG/DTA measurements, qualitative and quantitative analysis, examination
                                            standalone systems.                                                                       times. After the completion of the measurement, the cooling starts   of reaction mechanisms and evaluation of heat resistance are performed by
                                                                                                                                                                                         studying various reactions and interactions between a sample and special
                                                                                                                                      automatically and stops when the furnace has reached a preset temperature.
                                                                                                                                      Now the next analysis can be started. Cyclic and cooling runs are under full   atmospheres. The unique channel structure of the DTG-60 series offers the
                                            If  exibility and high performance is needed in various applications, the new             instrument control.                                solution for these applications. While an inert gas purges the balance, reactive
                                            DTG-60/60H combines them all: Basic functions required by simultaneous                                                                       gases are directly connected to the reaction pan.
                                            thermogravimetry/differential thermal analysis (TG/DTA) measurements are improved.
                                            Atmosphere control is programmable. As in DSC, the TA-60WS provides advanced                                                                                     Gas Out  Cleaning Gas In
                                            acquisition, analysis and report functions which ensure comfortable simultaneous
                                                                                                                                                                                                                    Gas In
                                            measurements.



            High sensitivity and high precision of balance is                                                                                                                                                        Solenoid
                                                                                                                                                                                                                     Valve
            equivalent to dedicated single-function instruments
            Model DTG-60 series has a unique balance mechanism (Roberval mechanism) that   The change in the center
            prevents changes in sensitivity from factors such as thermal expansion and allows high   of gravity does not matter.      Setting for the Cooling fan control parameter (Detector properties box)      Gas In
            precision thermogravimetric measurements. Furthermore, the fulcrum used for the                                                                                                                        Vacuum Pump
            balance is made from thin alloy metal strips that have tiny thermal coefficients and are
            crossed to form an "x" shape. This fulcrum (X-shaped fulcrum) is lightweight and has
            extremely low friction and resistance. Using this fulcrum configuration allows   The load is applied at
            incorporating a highly sensitive balance and is even highly resistant to vibration.  the same point no matter
                                                                                            where the sample is placed.               DTG-60A/60AH provides a                            High sensitivity DTA detectors
                                                                                                                                      compact built-in autosampler
                                                                                                                                      Up to 24 samples can be setup for analysis. In addition, the weight of empty
                        TGA                       DTA
                        mg                        µV                                                                                  cell and sample can be measured automatically.
                         TG  −12.353%
                      0.0
                                      −19.020%
                                                     100.0
                                            −30.196%
                     −0.5
                         DTA                         0.0
                     −1.0
                                               679.05˚C                     X-Shaped Fulcrum
                             164.75˚C
                            200.0  400.0  600.0  800.0
                                    Temp [˚C]

                           Measurement of trace CaC2O4
                                                                 Furnace
                                                                                                                                      Specifications
                        TGA                       DTA             Sample
                        mg                        µV              Holder                                                                                             DTG-60            DTG-60H            DTG-60A           DTG-60AH
                                           Rubber                                                                                       Balance principle                               Parallel guide differential top pan type
                      0.0  TG              Substances  2000                                                                             Temperature range        Ambient to 1100℃   Ambient to 1500℃   Ambient to 1100℃   Ambient to 1500℃
                                           −68.281%
                    −10.0                  Carbon Black                                     Furnace Base                                Measurable range (TG)                                    ±500mg
                                           −28.158%                                                                                     Measurable range (DTA)                                   ±1000µV
                                          ↑          1000        Beam
                    −20.0          Switches from                                            Joint Section                               Weight readability                                        0.1µg
                                   nitrogen to air                Shutter                                                               Sample quantity                                     1g Max. in gross weight
                    −30.0                                                                   Coil                                        Atmosphere                                             Air and inert gas
                         DTA                         0                                                                                  Auto sampler                            ─                                24 samples / tray
                    −40.0                                                                     Magnet                                    Standard sample                         ─                                   Fixed
                        0.0  200.0  400.0  600.0  800.0                                    X-Shaped Fulcrum                             Analysis / Print                        ─                       Automatic analysis and automatic report printout
                                   Temp [˚C]                                             Photoelectric                                  Size                                                W 367×D 650×H 453mm
                                                                                         Conversion Element
                           Measurement of carbon black in SBR                        Lamp                                               Weight                                 35kg                                  40kg
                                                                                                                                                                AC 100 V, 120 V, 230 V,  AC 100 V, 120 V, 230 V,  AC 100 V, 120 V, 230 V,  AC 100 V, 120 V, 230 V,
                                                                                                                                        Power supplySpecifications
                                                                                                                                                                 1300 VA, 50/60 Hz  1500 VA, 50/60 Hz  1300 VA, 50/60 Hz  1500 VA, 50/60 Hz

                                                                                                                                                                                                                                  60 Series
      4                                                                                                                                                                                                                      Thermal Analysis Instruments  5
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