Page 156 - Shimadu Consumables Catalog
P. 156

GC Columns



           Capillary Columns
           High-Performance Columns


              SH-I-1MS
              Non-polar phase: Crossbond™ 100% dimethyl polysiloxane
                                                                                          SH-I-1MS  Structure
              Tested and guaranteed for ultra-low bleed; improved signal-to-noise ratio for better sensitivity
             and mass spectral integrity.
              General-purpose columns for arson accelerants, essential oils, hydrocarbons, pesticides, PCB
             congeners (e.g., Aroclor mixes), sulfur compounds, amines, solvent impurities, simulated
             distillation, oxygenates, gasoline range organics (GRO), refinery gases.
              Equivalent to USP G2 phase.

              Similar phases: HP-1ms UI, HP-1ms, DB-1ms UI, DB-1ms, Ultra-1, VF-1ms, SPB-1, Equity-1

              ID         df          Temp. Range          20 m                25 m                 50 m
                       0.15 µm     -60 to 330/350 °C   227-36001-01             −                   −
            0.15 mm
                       2.00 µm     -60 to 330/350 °C   227-36002-01             −                   −
                       0.18 µm     -60 to 330/350 °C   221-75921-20             −                   −
            0.18 mm
                       0.36 µm     -60 to 330/350 °C   227-36003-01             −                   −
            0.20 mm    0.33 µm     -60 to 330/350 °C       −                227-36004-01        227-36004-02
              ID         df          Temp. Range          15 m                30 m                 60 m
                       0.25 µm     -60 to 330/350 °C   227-36005-01         221-75923-30        227-36005-02
            0.25 mm    0.50 µm     -60 to 330/350 °C   227-36006-01         227-36006-02        221-75924-60
                       1.00 µm     -60 to 330/350 °C   227-36007-01         227-36007-02        227-36007-03
                       0.25 µm     -60 to 330/350 °C   227-36008-01         221-75926-30        227-36008-02
                       0.50 µm     -60 to 330/350 °C   227-36009-01         227-36009-02        227-36009-03
            0.32 mm
                       1.00 µm     -60 to 330/350 °C       −                227-36010-01        221-75928-60
                       4.00 µm     -60 to 330/350 °C       −                227-36011-01            −
                       0.50 µm     -60 to 330/350 °C   227-36012-01         227-36012-02            −
            0.53 mm    1.00 µm     -60 to 330/350 °C   227-36013-01         227-36013-02            −
                       1.50 µm     -60 to 330/350 °C   227-36014-01         227-36014-02        227-36014-03

           Petroleum Hydrocarbons (TPH)
                                                                     Peaks   Conditions
                                                                   1.   C8  Instrument  :  GC-2010
                                                                   2.   C10  Column   :  SH-I-1Ms, 20 m,
                                                                   3.   C12             0.18 mm ID, 0.18 μm
                                                                   4.   C14             (P/N: 221-75921-20)
                                                                   5.   C16
                                                                   6.   C18  Sample   :  Florida TRPH Standard, 500 μg/mL
                                                                   7.   C20             each component in hexane
                                                                   8.   C22  Inj. Vol.          :  0.5 μL, split (split ratio 20:1)
                                                                   9.   C24  Inj. Temp   :  275 °C
                                                                   10.   C26  Carrier Gas   :  Hydrogen, constant
                                                                   11.   C28            linear velocity mode,
                                                                   12.   C30
                                                                   13.   C32            55 cm/sec.
                                                                   14.   C34  Oven Temp   :  40 °C (hold 1 min) to
                                                                   15.   C36            330 °C at 20 °C/min
                                                                   16.   C38            (hold 10 min)
                                                                   17.   C40  Detector  :  FID, 350 °C













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