Page 5 - Shimadzu-FoodSafety

Analysis of Residual Pesticides Analysis of Residual Pesticides

Food knows no borders. With an increasing global population, food security is increasingly under threat and there is a Simultaneous Analysis of Residual Pesticides (GC-MS/MS) Triple Quadrupole Mass Spectrometer
growing challenge for agriculture to produce more food, safely and more sustainably. The use of herbicides, insecticides, and GCMS-TQ8050
(×1,000,000)
fungicides reduce crop losses both before and after harvest, and increase crop yields. However, pesticide residues resulting
7.0
from the use of plant protection products on crops may pose a risk to human health; as a result, regulatory guidelines have 6.0
been implemented to monitor pesticide residues in food. Shimadzu offers a wide range of instruments for pesticide testing, 5.0
from GC and LC with specific detectors to single and triple quadrupole mass spectrometers. 4.0
3.0
2.0
Triple Quadrupole Mass Spectrometer Simultaneous Analysis of Residual Pesticides (LC-MS/MS) 1.0
LCMS-8060 5.0 7.5 10.0 12.5 15.0 17.5 20.0 22.5
LC-MS/MS MRM (Multiple Reaction Monitoring) analysis allows
for rapid and sensitive detection of pesticides in complex Simultaneous Analysis of 439 Pesticides Using GC-MS/MS with Smart MRM
matrices. An example of simultaneous multi-residue multi-class
Source: Shimadzu Application Data Sheet No. C106, 107
pesticide analysis is shown below.
Finally, a triple quadrupole GC-MS/MS Smart enough for everyday use in your laboratory. The Shimadzu GCMS-TQ8050 is the
(x1,000,000) first triple quadrupole with Smart Productivity for high-efficiency sample throughput, Smart Operation for quick and easy
2.00 method development, and Smart Performance for low detection limits and Scan/MRM. These three smart technologies
contribute to Smart MRM and provide the most accurate, cost-effective, and easy-to-use triple quadrupole GCMS you have
1.75
ever imagined.
1.50
1.25
Database
1.00
The LCMS-8060 is a groundbreaking innovation in mass 0.75 Database for Quantitative Analysis
spectrometry, helping to transform LC-MS/MS data quality by 0.50 Smart Pesticides Database
developing a new vision of sensitivity and speed. 0.25 The Smart Pesticides Database includes optimized transitions and
collision energies, CAS registry numbers, and Retention Indices (RI)
Shimadzu is the first mass spectrometry company in the 0 for hundreds of pesticides. Select from pre-registered compounds in
world to deliver a triple quadrupole mass spectrometer with 0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 min one database, or add you own optimized transitions. Select the
the highest sensitivity and ultra-fast technologies. Simultaneous Analysis of 646 Pesticides (10ng/mL) within 10.5 minutes Using LC-MS/MS compounds to be analyzed, and Smart MRM builds the MRM or
Scan/MRM acquisition method from the “Smart Database” with a
push of a button.
Database Peak Area Response
Quantitation Ion Database for Screening Analysis
×10 6
LC/MS/MS Method Package for Residual Pesticides 5.0 APPLE MINT TOMATO Quick-DB*
The Method Package covers 836 components subject to EU Directive 4.5 %RSD 3.7 MS Residual Pesticides Database
No. 396/2005, Chinese GB standards, and the Japanese Multi-residue 4.0 In pesticide analysis, increased purchasing costs and the control
%RSD 3.4 %RSD 3.4 Dipropetryn
Method for Agricultural Chemicals by LC-MS/MS. In the USA, the EPA 3.5 operations associated with standard samples have become issues for
sets the pesticide limits while the FDA and USDA enforce those limits. 3.0 the industry. The Quick-DB contains information on 491
The method package also includes optimized analytical conditions, 2.5 components, optimized analytical conditions, and calibration curves
%RSD 3.9
which enables simultaneous analysis of 646 pesticides in 10.5 minutes 2.0 %RSD 3.2 Probenazole created using pesticide surrogates as internal standard substances.
without performing a complicated conditions setting process. 1.5 %RSD 3.6 This allows quick screening of residual pesticides without using
1.0 %RSD 5.4 %RSD 5.9 Thiofanox-sulfone pesticide standard samples.
%RSD 5.8
0.5 *Not available in the USA
Registered
Method File Mode 0.0
Component 0 50 100 150 200 250 300
Injections number
Pesticide MRM 836 Thiofanox-sulfone Dipropetryn Probenazole Multi-Analyte Quantitation Software
LabSolutions Insight
Peak Area Response for Three Pesticides Spiked into Apple, Mint and Tomato
Matrix Extracts at 0.05 mg/kg over 72 Hours.
Due to increasingly sophisticated automation, large quantities
Source: Shimadzu Application News No. C136 of high-quality mass spectrometer data can be obtained.
However, checking and analyzing all that data can be extremely
time-consuming, which significantly decreases the efficiency of
inspection work. LabSolutions Insight multi-analyte quantitation
software for GC-MS/MS and LC-MS/MS analysis helps analyze
such multi-analyte data more conveniently and more efficiently.
s T
otal Support for Food Safety
Shimadzu’
Shimadzu’s Total Support for Food Safety
4 Analytical and Testing Instruments for Food Safety 5