Page 6 - Shimadzu AIM-9000
P. 6

Automatic  Automatic
                                                                                                                                                                                                                  Contaminant  Qualitative
                                                                                                                                                                                                                  Recognition  Analysis
                     Functionality That Is Simpler and                                                                                                                                                   Wide-Field  Finally, a wide view   Sensitivity
                                                                                                                                                                                                                                         High
                                                                                                                                                                                                          Camera
                                                                                                                                                                                                                   on micro sample analysis
                     More Convenient to Use
                                                                                                                                                                                                            Contaminant             Micro
                                                                                                                                                                                                              Analysis   Surface    Analysis
                                                                                                                                                                                                                         Analysis






                       Perform Infrared Measurements Smoothly                                                                              Perform Ultra Micro Analysis   - Best-in-Class Signal-to-Noise Ratio -
                       While Viewing Visible Images
                       - Visible/Infrared Dual View System -                                                                            The AIM-9000 optimized for measuring extremely small areas. The AIM-9000 achieves 30,000:1 signal-to-noise ratios, the best in its
                                                                                                                                        class. Consequently, it can quickly obtain excellent spectra from even extremely small contaminants.
                     Infrared spectra can be measured while checking a visible                                                          Transmission measurement of
                                                                                                                                                                                                  AIM-9000  Display peak intensity
                     image of the sample. Spectra can be measured while                                                                 polystyrene beads                                         Previous   after modifying to
                                                                                                                                                                                                  model  appropriate scale
                     confirming the position of contaminants, which avoids the                                                          A ø10 µm polystyrene bead was                                Abs
                     trouble of switching back and forth between the visible                                                            measured by transmittance method.
                     light and infrared light.                                                                                          Low noise and a high-quality                        Abs
                                                                                                                                                                                                      4000     3200     2400  2000
                     Used in combination with the tiling function, visible                                                              spectrum of a very small sample                                                      cm -1
                     observations and infrared measurements can be performed                                                            were obtained with only a small   Sample   : 10 µm diameter polystyrene
                                                                                                                                                                             bead on BaF2 window plate
                     anywhere within the stage operating range, eliminating the                                                         number of scans.           Measurement
                     need to reposition the sample.                                                                                                                Condition   : Aperture size 15 × 15 µm
                                                                                                                                                                   Number of Scans  : 40 (about 20 seconds)
                                                                                                                                                                                             4000  3200  2400  1800  1400  1000  cm -1
                                    Image view of the visible light and infrared optical path
                                             Green light: visible light optical path
                                             Red light: infrared optical path                                                              Perform High-Sensitivity ATR Measurement   - Samples with High Refractive Index -
                                                                                                                                        The Ge prism (P/N 206-32600-41) has an anti-reflective coating that provides high sensitivity.
                       Visualize Components   - Chemical Imaging  -                                                                     Due to a steeper incident angle for the infrared light, compared to the previous model, the AIM-9000 is able to acquire
                                                                     *
                                                                                                                                        excellent distortion-free ATR spectra even when measuring samples with a high refractive index, such as black rubber.
                     The invisible distribution of chemicals can be visualized based on peak height or area, multivariate analysis (PCR/MCR), or                                                             0.5
                                                                                                                                        ATR measurement of black
                     spectral similarity to target spectra.                                                                                                                                         AIM-9000  Abs
                                                                                                                                        rubber                                                0.6
                                                                                                                                                                                                    Previous model  0.4
                     Chemical image of pharmaceutical powder                                                                            An acrylonitrilebutadiene rubber
                     Pharmaceutical products were rolled with a diamond cell, then                                                      (NBR) with 50 wt% carbon was                          0.4               1000  800
                                                                                                                                                                                                                      cm -1
                     mapping measurement was performed.                                                                                 measured by Ge-ATR objective. A                     Abs
                     Right figure represents the distribution of powder components,                                                     clear peak of C=C-H out-of-plane
                     such as lactose, lipid, and cellulose.                              Distribution of lactose                                                   Sample   : NBR with 50 wt%   0.2
                     Color display can be switched freely between single-color and       O-H stretching                                 bending mode was obtained at          carbon content
                     multi-color.                                                        (Around 3526 cm -1 )                           970 cm , which was strained by   Measurement
                                                                                                                                             -1
                                                                                                                                                                   Condition   : Aperture size 50 × 50 µm
                                                                                                                                        conventional ATR objective.  Number of Scans  : 20 (about 10 seconds)  0.0
                                                                                                                                                                                               4000   3000   2000   1500  1000  cm -1
                                                                                                                                           Fully Support Identification of Contaminants
                                                                                         Distribution of lipid                             - Contaminant Library for LabSolutions IR and Thermal-Damaged Plastics Library  -
                                                                                                                                                                                                                          *
                                                                                         C-H stretching
                                                                                         (Around 2855 cm -1 )
                                                                                                                                        Contaminant Library for LabSolutions IR (P/N 206-33179-91)
                                                                                                                                        This unique library was created by Shimadzu especially for analyzing contaminants in tap water and food products. The library
                                                                                                                                        includes information about samples actually collected as contaminants and service parts commercially marketed for tap water
                                                                                                                                        applications. It also includes a collection of X-ray fluorescence profiles (PDF files). Consequently, it can significantly improve the
                                                                                                                                        precision of contaminant searches. Unlike previous libraries, this is a mixture library that covers the extensive knowledge and
                                                                                         Distribution of cellulose
                                                                                         C-O stretching                                 experience necessary for qualitative analysis.
                                                                                         (Around 1060 cm -1 )
                                                                                                                                        Thermal-Damaged Plastics Library (P/N 206-33039-91)
                                                                                                                                        This unique library includes information about plastics that have degraded due to oxidation by heating. The library is especially
                      Microscopic image of pharmaceutical powder
                                                                                                                                        useful for analyzing degraded contaminant substances, which are common.
                                                                   * Visualizing chemicals requires an optional mapping program (P/N 206-32936-41).
                                                                                                                                                     * Shimadzu created the library using spectra obtained by Hamamatsu Technical Support Center, Industrial Research Institute of Shizuoka Prefecture.




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