Page 11 - 4_TOC special applications
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SCA-130-404






        ▪ Calibration                                         ▪ Results
        The instrument was calibrated using a potassium       The analysis of the different water types using the
        hydrogen phthalate stock solution, using the          NPOC method yielded meaningful results within a
        automatic     dilution   function,   at    carbon     few minutes. All TOC concentrations were within a
        concentrations of 0, 0,3, 1,0, 2,0 and 3,0 mg/L       low range between 0,004 and 0,3mg/L, but could
        (Fig1.). In order to eliminate the influence of       be determined with very low standard deviations
        carbon impurities in the ultra pure water used to     (Fig.3).
        prepare the standard solutions, the calibration
        curve   was   shifted  in  parallel  through   the
        coordinate origin.                                       Sample                     NPOC     SD
                                                                                            [mg/l]   [mg/l]
                                                                 Table water                0,108    0,003

                                                                 Deep well water            0,042    0,006
                                                                 Spring water               0,063    0,002

                                                                 Natural mineral water      0,281    0,001
        Fig.1: 5-point calibration in range 0 to 3mg/L
                                                              Fig.3: NPOC-Concentrations of the various water types

        ▪ Method parameters
        Method:               NPOC                            TOC    analysis  allows   the  manufacturers    of
                                                              beverages to easily and quickly assess the content
        Acidification:        1,5%                            of organic contaminants in their feedstock, thus
        Injection volume:     1.000µl                         helping to optimize production processes and
        Sparge time:          1,5min (in the syringe)         further ensure product quality.
        No. of Injections:    3 / Max. 5


                                                              ▪ Recommended instrument / configuration
                                                              TOC-L  CPH
                                                              ASI-L










        Fig.2: 3 NPOC-Injections of spring water




















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