Page 14 - Shimadzu Nexera UC

SFE Pretreatment System Shim-pack ™ UC Series

This system allows the pretreatment of samples using supercritical fluid. An extraction operation that changes the types of
modifiers (up to four types) and concentrations to mix with supercritical carbon dioxide can be performed on each sample. The In the analysis with supercritical fluid chromatograph system Nexera UC, because diffusion of the sample band
extracted material is collected in a test tube using a FRC-40 SF fraction collector. The LotusStream separator allows fractionation
of small volumes, even into vessels such as 1.5 mL vials, without dispersion of the solvent. In addition to analysis by SFC, the system in mobile phase is high compared with liquid chromatography, separation behavior changes significantly due
is ideal for measurements using other analytical systems such as GCMS and NMR. to different types of columns.
Shim-pack UC series was designed with variety types of stationary phases which making it suitable for the
mobile phase of high diffusion and low viscosity liquid carbon dioxide.

˙ Achieve high speed and high performance by utilizing the features of Nexera UC

˙ Wide range of stationary phases meets diverse needs

˙ High durability and stable reproducibility

I.D. × L (mm) 3 µm 5 µm I.D. × L (mm) 3 µm 5 µm
2.1×150 227-30400-01 227-30402-01 2.1×150 227-32600-01 r
2.1×250 227-30400-02 227-30402-02 4.6×250 r 227-32600-02
Shim-pack UC-RP
4.6×150 227-30401-01 227-30403-01 Shim-pack UC-HyP 10×250 r 227-32600-03
4.6×250 227-30401-02 227-30403-02 20×250 r 227-32600-04
2.1×150 227-30404-01 227-30406-01 28×250 r 227-32600-05
2.1×250 227-30404-02 227-30406-02 2.1×150 227-32601-01 r
Shim-pack UC-GISᶘ
4.6×150 227-30405-01 227-30407-01 4.6×250 r 227-32601-02
4.6×250 227-30405-02 227-30407-02 Shim-pack UC-Py 10×250 r 227-32601-03
2.1×150 227-30408-01 227-30410-01 20×250 r 227-32601-04
2.1×250 227-30408-02 227-30410-02 28×250 r 227-32601-05
Shim-pack UC-Diol
Chiral Screening System SFC-UV System 4.6×150 227-30409-01 227-30411-01 2.1×150 227-32602-01 227-32602-02
r
r
227-30409-02 227-30411-02
4.6×250
4.6×250
2.1×150 227-32606-01 – Shim-pack UC-PBr 10×250 r 227-32602-03
This system is best for developing methods to separate chiral This is the minimum setup of Nexera UC and is suitable to 4.6×250 – 227-32606-02 20×250 r 227-32602-04
compounds. replace both normal phase and reverse phase LCs. A wide Shim-pack UC-Diolᶘ 10×250 – 227-32606-03 28×250 r 227-32602-05
It automatically generates a large number of methods by range of analyte polarity can be covered by the combination of 20×250 – 227-32606-04 2.1×150 227-32603-01 r
utilizing combinations of up to 12 columns, four modifiers, and supercritical fluid and modifiers (for example, MeOH). 28×250 – 227-32606-05 4.6×250 r 227-32603-02
a different ratio of modifiers to mobile phase. Hazardous organic solvents such as hexane or chloroform are 2.1×150 227-30412-01 227-30414-01 Shim-pack UC-Choles 10×250 r 227-32603-03
eliminated. This system reduces environmental impact by Shim-pack UC-Sil 2.1×250 227-30412-02 227-30414-02 20×250 r 227-32603-04
r
28×250
utilizing low-toxicity mobile phases and completing analyses in 4.6×150 227-30413-01 227-30415-01 2.1×150 227-32604-01 227-32603-05
227-30413-02 227-30415-02
4.6×250
r
a shorter time. 2.1×150 227-32607-01 – 4.6×250 r 227-32604-02
4.6×250 – 227-32607-02 Shim-pack UC-PyE 10×250 r 227-32604-03
Shim-pack UC-Silᶘ 10×250 – 227-32607-03 20×250 r 227-32604-04
20×250 – 227-32607-04 28×250 r 227-32604-05
28×250 – 227-32607-05 2.1×150 227-32605-01 r
2.1×150 227-30416-01 227-30418-01 4.6×250 r 227-32605-02
2.1×250 227-30416-02 227-30418-02 Shim-pack UC-Triazole 10×250 r 227-32605-03
Shim-pack UC-Amide
4.6×150 227-30417-01 227-30419-01 20×250 r 227-32605-04
4.6×250 227-30417-02 227-30419-02 28×250 r 227-32605-05
2.1×150 227-30420-01 227-30422-01 Shim-pack UC-Diolᶘ(G) 10×20 r 227-32606-06
2.1×250 227-30420-02 227-30422-02 Shim-pack UC-Silᶘ(G) 10×20 r 227-32607-06
Shim-pack UC-NH2
4.6×150 227-30421-01 227-30423-01 Shim-pack UC-HyP(G) 10×20 r 227-32600-06
4.6×250 227-30421-02 227-30423-02 Shim-pack UC-Py(G) 10×20 r 227-32601-06
2.1×150 227-30424-01 227-30426-01 Shim-pack UC-PBr(G) 10×20 r 227-32602-06
2.1×250 227-30424-02 227-30426-02 Shim-pack UC-Choles(G) 10×20 r 227-32603-06
Shim-pack UC-Phenyl
4.6×150 227-30425-01 227-30427-01 Shim-pack UC-PyE(G) 10×20 r 227-32604-06
4.6×250 227-30425-02 227-30427-02 Shim-pack UC-Triazole(G) 10×20 r 227-32605-06
2.1×150 227-30428-01 227-30430-01 Column Pressure Capacity
2.1×250 227-30428-02 227-30430-02
Shim-pack UC-CN • 3 m particle diameter: 50 MPa
4.6×150 227-30429-01 227-30431-01 • 5 m particle diameter (with 2.1 to 10 mm I.D.): 30 MPa
4.6×250 227-30429-02 227-30431-02 • 5 m particle diameter (with 20 to 28 mm I.D.): 23 MPa
Nexera UC
14 Supercritical Fluid Extraction/Chromatograph System 15