Page 72 - Shimadu Consumables Catalog
P. 72

UHPLC/HPLC Columns



           Shim-pack FC-ODS

           High-speed analysis of 2,4-DNPH derivatized aldehydes / ketones














                                     Conditions
                                    Column    :  Shim-pack FC-ODS (75 mmL. × 4.6 mmI.D., 3 μm)
                                                (P/N: 228-40511-92)
                                    Mobile Phase  :  Water/Acetonitrile = 55/45 (v/v)
                                    Flow Rate   :  1.0 mL/min
                                    Col. Temp.   :  40 °C
                                    Detection   :  UV 360 nm
           Chromatogram of Standard Sample                                       Chromatograms of Environmental Air (A)
           (formaldehyde 0.35μg/mL, acetaldehyde                                 and Indoor Air at Laboratory (B)
           0.55μg/mL, 10μL injected)










                                            Conditions
                                          Column    :  Shim-pack FC-ODS
                                                      (75 mmL. × 4.6 mmI.D., 3 μm)
                                                      (P/N: 228-40511-92)
                                          Mobile Phase  :  A) Water/Tetrahydrofuran = 8/2 (v/v)
                                                      B)  Acetonitrile
                                                      A/B = 80/20 - 14min - 40/60 - 0.01min -
                                                      80/20 - 6min
                                          Flow Rate   :  1.2 mL/min
                                          Col. Temp.   :  40 °C
                                          Detection   :  UV 365 nm
           Chromatogram of Standard Sample                                       Chromatograms of Indoor Air at Laboratory (A)
           (each 0.3 ug/mL as carbonyl compounds, 10uL                           and Operation blank (B)
           injection)

              Product Information

              Particle Size       I.D. (mm)     2.0            4.6
                (μm)     Length (mm)
                                30              -           228-40511-91
                 3              75          228-40511-94    228-40511-92
                               150          228-40511-95    228-40511-93





















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