Page 4 - ICPMS-2040 Series
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Exceptional yet Eco Friendly



                     An advanced mini-torch design, combined with a redesigned collision/reaction cell, and a high-perfor-
                     mance  quadrupole mass filter  result  in  an environmentally  friendly  system with superior analytical
                     performance.                                                                                                       Redesigned Collision/Reaction Cell                                          Product


                                                                                                                                        Collision Mode

                                                                                                                                        Inert helium gas is introduced into the cell to selectively attenuate kinetic energies of polyatomic ions
                                                                                                                                        based on their sizes. These low energy ions are removed from the ion beam by applying a bias voltage at
                                                                                                                                        the cell exit. Because fewer by-product ions are generated, it can be used for a wide range of applications.


                                  Quadrupole Mass Filter                Collision/Reaction Cell  Mini-Torch System
                                                                                                                                        Online Interelement Correction (IEC)

                     Proprietary Advanced Mini-Torch System                                                                             Shimadzu’s proprietary online interelement correction (IEC) function is used to correct for spectral
                                                                                                                                        interference that cannot be eliminated by the collision mode. By only measuring one standard sample
                                                                                                                                        an interference correction is calculated and applied to all samples run subsequently.
                                                                                  ~2 times higher
                     Redeveloped High Sensitivity                                   sensitivity
                     Mini-Torch                                 New design
                                                                                                                                        Reaction Mode
                     Optimizing the torch design keeps argon gas                                  Wide
                     consumption low and decreases sample flow                                                                          When a specific gas is introduced into the cell, the reaction of gas with ions is used to reduce
                     rate into the plasma, improving sample                                                                             interferences. Target ions can be analyzed with high sensitivity, while both doubly charged ions not
                                                                 Plasma temperature = 7500 K
                     ionization efficiency. The new design roughly                          Injector bore diameter                      eliminated by the collision mode and polyatomic ions can be reduced.
                     doubles sensitivity compared to previous   Previous design
                     models while reducing injector clogging
                     issues.                                                                     Narrow                                    Quadrupole Mass Filter    Collision/Reaction Cell  Interface
                                                                                                                                                                                           Region
                                                                                                                                                                                                         Target ion       78 Se +

                                                                                                                                                                                                         Doubly charged ion  156 Gd 2+
                                                                                                                                         m/z=78                                                          Polyatomic ion  40  38  +
                                                                                        0     10     20                                                                                                                  Ar Ar
                     Low Argon Gas Consumption                                                                                                     m/z=156
                                                                                                                                                                                                         Reaction gas      H2
                     A major drawback of ICP-MS systems is the large argon   Typical ICP-MS system
                                                                         (18 L/min flowrate)
                     gas consumption. Shimadzu’s mini-torch system
                     consumes 11 L/min of argon, two-thirds the amount   ICPMS-2040/2050 Series
                     used by typical plasma torches. Continuous operation   (Mini Torch)                                                Note: Example of how reaction mode can be used. Reaction gas H2 is used in this example to convert doubly-charged ions to singly-charged ions,
                                                                                                                                        and charged polyatomic ions to neutral clusters.
                     using a 7 m  gas cylinder is up to 10 hours. Utilizing   ICPMS-2040/2050 Series
                               3
                     Eco mode (5.5 L/min plasma) during standby can      (Eco Mode)
                     further reduce argon gas consumption.
                                                                                           Total Gas Flowrate (L/min)
                                                                                                                                        High-Performance Quadrupole Mass Filter



                                                                                                                                        Charge Stabilizer
                                                                                                 Reduction in gas
                                                                                                   consumption
                     No Need for High-Purity Argon Gas                                          Use of low-purity gas
                                                                                                                                        To mitigate ion charge effects on the mass filter, a pulse voltage is applied between the analysis of
                     ICPMS-2040/2050 Series systems have a Shimadzu-made                                                                each mass to maintain a constant charge level at the electrode surface. This improves the signal
                     high-frequency power supply that features high-speed                                                               stability when analyzing samples for long periods (patent pending).
                                                                               Typical ICP-MS system  ICPMS-2040/2050 Series
                     matching functionality, allowing for the use of low-cost,   (99.999 % purity at   (99.99 % purity at
                     low-purity (99.95 %) argon gas to reliably generate a      18 L/min flowrate)  11 L/min flowrate)
                     robust plasma.                                                 Argon Gas Cost Reduction                            High-Resolution Mode and Half-Mass Correction
                                                                              Note: The reduction in cost will vary according to
                                                                              current gas pricing. This calculation assumes the         Masses can be analyzed at 0.5 u intervals using high-resolution mode, enabling half-mass correction for
                                                                              price of 99.999% purity argon is two times higher
                                                                              than the price of 99.99% purity.                          doubly charged interferences common in rare earth elements (REEs).



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