Page 25 - Food&Beverages Solutions-for-EtO-Analysis-SSI

3.1, 3.2 & 3.3 Ayurveda Samples (Liquid & Dynamic Headspace)
Amala, Ashwagandha, Boswellia Serrata Powder

Application Databook

EtO & 2-CE Analysis In Ayurveda / Herbal Samples (Extracted solution In Headspace Vial)

APPROACH MODE OF ANALYSIS INJECTOR INSTRUMENT TECHNIQUE

3.1 Amala Powder Sample
st
Headspace – Method 1 (EtO & 2-CE) Dynamic Headspace SPL HS-20 NX - GCMS-TQ8050 NX

APPROACH MODE OF ANALYSIS INJECTOR INSTRUMENT TECHNIQUE

3.2 Ashwagandha Powder Sample

st
Headspace – Method 1 (EtO & 2-CE) Dynamic Headspace SPL HS-20 NX - GCMS-TQ8050 NX

¿ This section deals with various approaches, extraction process & different instrument
techniques used for the analysis of EtO and 2-CE in Boswellia Serrata powder sample

APPROACH MODE OF ANALYSIS INJECTOR INSTRUMENT TECHNIQUE

3.3 Boswellia Serrata Powder Sample

st
Headspace – Method 1 (EtO & 2-CE) Dynamic Headspace SPL HS-20 NX - GCMS-TQ8050 NX
EURL-SRM Analytical Observation Liquid SPL AOC-20i/s - GCMS-TQ8050 NX
Report (EtO & 2-CE)

System Description

GCMS System GCMS-TQ8050 NX
Headspace Sampler HS-20 NX (Dynamic Headspace)
Capillary Column RTX-VMS (60 m X 0.45 mm ID x 2.55 um df)
Ionization Mode Electron Ionization (EI)
Sample Information EtO & 2-CE in Ayurveda & Herbal Samples

Benefits

Ÿ Shimadzu have developed dynamic headspace methods for the analysis of EtO & 2-CE in spices
matrix. This method outperforms the current regulatory limits.
Ÿ Shimadzu’s GCMS-TQ8040 NX / GCMS-TQ8050 NX with liquid autosampler & dynamic headspace
sampler is complete tool for the analysis of EtO & 2-CE.

25