Page 9 - Food&Beverages Solution Palm Oil
P. 9

Atomic Absorption Spectrophotometer (AAS)  Fourier Transform Infrared Spectrophotometer (FTIR)






 Dimethylpolysiloxanes  Trans Fatty Acids

 Dimethylpolysiloxanes or methyl silicones are commonly added to fats and oils to prevent oxidative foaming in products used in frying   Trans fatty acids are a kind of fat that is found in foods. Excessive ingestion of this type of fat is associated with elevated low density
 applications. To measure the amount of Dimethylpolysiloxanes, a direct aspiration, flame atomic absorption method is used.  lipoprotein (LDL) cholesterol levels, which increases the risk of heart disease. Food entrepreneurs have been taking measures for some
            time by independently developing low trans fatty acid foods and selling them on the market. At the same time, nations such as the
 Instrument Optics Parameters  United States and Denmark are obligated to display the trans fatty acid content on food labels and to adhere to content restrictions
 Equipment   :Atomic Absorption Spectrophotometer   Measurement wavelength (nm) :251.6   on trans fatty acids.
     AA-7000F   Slit width (nm)   :0.7
 Lamp current (mA)  : 20   BGC mode   :BGC-D2
            Shown here is a quantitative analysis study conducted for trans fatty acids by the ATR and transmission methods. Measurement was
            conducted according to the official method as prescribed by The American Oil Chemists' Society (AOCS). Measurement was also conducted
 Results and Repeatability
            by the transmission method in cases where the trans fatty acid content was assumed to be very low.


                                                                  Corr. Height
                                                                  0.225
                                                                  0.25
                                                                  0.225
                                                                   0.2
            Analytical Conditions                                 0.175
            Instrument  :IRPrestige-21                            0.15
                      with MIRacle A (heating plate)              0.125
            Resolution   :4 cm  -1                                 0.1
 Calibration curve generated from DMPS standards  Accumulation :45  0.075
            Detector  :DLATGS
 Shimadzu Atomic Absorption Spectrophotometer Product Lineup      0.05
                                                                  0.025
 Model  Features                                                        0  1  2   3  4  5  6  7  8  9  10
                                                                                           r=0.9999  Concentration%
 · Double beam optical system                                   Calibration Curve of Trans Fatty Acid by Single Reflection ATR Spectroscopy
 · Provides superior baseline stability expected from high performance optical systems at an affordable price.
 · Two lamps simultaneously lit (manual turret)
 · Uses the least linear bench space of any atomic absorption spectrophotometer in the world.
 · User-friendly software with Wizard functions provides easy operation
 AA-6200          2  Trielaidin (non-spiked)      ―
                     Trielaidin (10.0% spiked)  ―
                Abs                                                Abs                     Trielaidin (10.0% spiked)
 ·Shimadzu's atomic absorption spectrophotometer with excellent cost effectiveness.  1.5
 ·Supports a wide range of analysis applications in fields such as environmental, chemistry, food etc.
 ·8-lamp turret
 ·Intuitive user-friendly software  1
 ·Trace Element Analysis by using Micro Sampling Technology
 AA-6880         0.5


 ·Features high-sensitivity analysis, flexible system configuration, space-saving and energy-saving design for   0  Trielaidin (non-spiked)
  user-friendly operation.
 ·First AAs to employ a vibration sensor as standard.   4000  3000  2000  1500  1000  750  500  1000  990  980  970  960  950  940  930
 ·Newly developed 3D double-beam optics ensure maximum performance for each measurement   1/cm            1/cm
  method through optimal adjustment of the light beam and light beam digital filter, and by using optical
  components that restrict light losses.  Infrared Spectra of Unspiked Olive Oil and Olive Oil Spiked with Trielaidin  Trans Fatty Acid Peak Region Selected for Calibration Curve
 ·Advances in optics and a new graphite furnace design achieve improved lower limits of detection for
  furnace analysis. Superb analysis performance is possible in all fields.
 AA-7000  ·Advanced safety technology
 ·Trace Element Analysis by using Micro Sampling Technology
 Reference: Determination of Dimethylpolysiloxanes in Oils Atomic Absorption Spectroscopy  Reference: Application News No. A430B Quantitative Analysis of Trans Fatty Acid by FTIR

                                          Solutions for Palm Oil Analysis Application Notebook
 8                                                                                                                   9
   4   5   6   7   8   9   10   11   12   13   14