Page 4 - Energy - Shimadzu Solution for Rechargeable Lithium-Ion Battery Evaluation

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Shimadzu Equipment for Evaluating Lithium-ion Rechargeable Batteries
Electrodes How the Lithium-ion Rechargeable Battery Works

Active Materials Binder

ICP Emission Spectrometer Sequential X-Ray Fluorescence Spectrometer High-Performance Liquid Chromatograph
ICP Series LAB CENTER XRF-1800 Prominence Series

Offers highly sensitive and accurate compositional analysis of materials and parts, Permits the non-destructive qualitative analysis of elements in different sample Prominence allows the separation and quantitation of organic substances and ions contained in the electrolyte
such as electrodes and electrolyte solution. states – solid, powder, or liquid. The FP method can conduct quantitative analysis solution.
An extensive lineup, from a multi-type system that features low running costs and without a calibration curve. It simplifies quantitation of battery constituent The extensive product range supports a wide range of analysis from ppb level to percentage level. In addition
quickly analyze. materials from major components to impurities, and provides comprehensive to concentration measurements, these instruments can measure the molecular weight distribution of polymers.
applications, including measurement of minute, 500 µm diameter regions.

Int.(Intensity) Infrared Microscope Measurement System Scanning Probe Microscope

IRTracer-100 SPM-9700HT
WL(Wavelength) Effective for the composition analysis of binders, electrolytes, and separators. The SPM-9600 easily takes high-magnification 3D images in air or liquid for
Spectral Line Profile The ATR method virtually eliminates the need for pretreatment and permits surface observations of samples from electrodes and semiconductors to separators
analysis of microscopic regions of a sample surface or thin film. The accuracy and and electrolyte membranes. Non-conductive objects do not require coating or
operability of the microscope system has been enhanced. other pretreatment. The instrument can measure the electrical characteristics of
Electron Probe Microanalyzer Nano Particle Size Analyzer the sample at the probe tip. Upgradeable to environment-controlled SPM.

EPMA-8050G SALD-7101
This instrument allows dispersion confirmation of the positive electrode materials Allows particle size distribution measurements in positive and negative active materials.
and observation of the distributions of binder and conduction enhancer. It can The SALD-7101 combines laser diffraction and scattering methods with a UV
also evaluate the deterioration of fuel cells by observing the behavior of fluorine in semiconductor laser (375 nm wavelength) to measure particle size distributions from
the solid polymer. The EPMA-8050G incorporates a high-resolution electron source 10 nm to 300 µm. Comprehensive options are available, including a high-concentration
for evaluation of the minute amounts of catalyst on the electrodes. sample measuring system and software to acquire data at 1 second intervals.

Electrolyte Solution (Solvent, Electrolyte, Additive)

Gas Chromatograph - Mass Spectrometer Gas Chromatograph

X-ray Diffractometer GCMS-QP2020 GC-2010Plus/2014 Series
ode material
oup: LIB, Data: Positive electr
Gr Group: LIB, Data: Positive electrode material
XRD-6100 This instrument is effective for composition analysis of electrolyte membranes, These instruments offer highly accurate and sensitive analysis of evolved gases
separators, and solvents in the electrolyte solution as well as for component and electrolytes. The GC-2010Plus/2014 supports both packed and capillary
X-ray diffractometry allows the qualitative analysis of crystalline analysis of emitted gases. columns to analyze a diverse range of samples. Excellent repeatability is
compounds. It can analyze the crystalline structure, orientation, In combination with pyrolysis, headspace, or other pretreatment methods, the assured by the optimized sample injection unit and the electronic flow
and size of positive and negative electrode active materials in the GCMS-QP2020 can analyze samples in different states. In addition to the controller (AFC) that accurately controls the carrier gas up to the
battery. It also offers qualitative analysis, crystallinity analysis, and commonly used electrospray ionization (EI), negative chemical ionization (NCI) is high-pressure, high-flow rate regions required for fast analysis.
orientation analysis of the separator material. Highly sensitive Diffraction Patterns of Positive Electrode Material available as an option to perform highly sensitive and selective analysis.
analysis using the polycapillary optical system is also possible. in a Lithium-ion Rechargeable Battery

KRATOS AXIS-Supra Imaging XPS System

AXIS-Supra
Permits observations of the composition and chemical status of materials on
the electrode and separator surfaces at nanometer-order resolution in the
depth direction. The XPS system can conduct measurements without
pretreatment, irrespective of the sample conductivity. It is effective for
evaluating materials characteristics and the degree of surface contamination.

Rechargeable Lithium-Ion Battery Evaluation
4 Analytical and Measuring Instruments for Rechargeable Lithium-ion Batteries 5