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Internal Combustion Engines                                                                                               Failure analysis and material control


            Evaluating Parts and Materials for Increasing the Temperature and                                                         Failure Analysis of Surface-hardened Gears
            Pressure of Engines and Exhaust Systems to Improve Fuel Efficiency                                                        – Hardness Distribution Evaluation and Fracture Origin Analysis by Carbon Content Mapping –

            - Testing Based on a Simulated Internal Engine Environment -
            Combustion efficiency is being improved by increasing the temperature and pressure inside the engine. Therefore, it is increasingly important to select or   Shafts, bearings, gears, and other automotive mechanical parts subject to high loads are often hardened, such as by high-frequency quenching, nitriding
            design materials that are suitable for high temperatures and pressures. In this example, thermal fatigue was evaluated to determine the performance of   or carburizing treatments, or coating technologies to improve their wear resistance and durability. Normally, quality is checked by measuring the depth of
            engine and exhaust system materials and the internal pressure fatigue was evaluated to assess pipes and other pressure-resistant parts.  the hardened layer. However, hardness can vary depending on the part shape and treatment conditions. Consequently, there is an increasing need to
                                                                                                                                      evaluate the hardness distribution. Similarly, hardness distribution evaluation is also being used to evaluate heat and pressure welded joints in more detail
              Evaluating Internal Pressure Fatigue                                                                                    than before. Typical hardness tests involve cutting out and testing part of the sample, but there is an increasing need to test the hardness in its unaltered

                                             Pressure amplifier                                                                       form. Hardness mapping is sometimes used for detailed analysis together with carbon content mapping. An example of a current topic in hardness
                                              mechanism
                                                                                                                                      testing and composition mapping that meets these needs is shown below.
                                                                                                                                        Evaluating Hardness Variations in Automotive Parts
                                                                           Pressure amplifier
                                                                            mechanism
                                                           Sample                                                                                                                        Surface


                                                                                                                                                                                         Cross
                        Electric-Hydraulic                        Pressurization                                                                                                         section
                        Fatigue Testing System                                       Depressurization                                                                                                          Evaluating the Depth of
                        EHF-U Series           Sample                                                                                                                                                          the Hardened Layer
                                             mounting port
                                                                                                                                                                                                               (JIS G 0559, ISO 3754)
            The pressure amplifier is used to apply pressure from inside the sample. Configured with special low-friction alloy bearings, precisely machined plungers, cylinders
            specially polished to improve durability, and a manifold, the system repeatedly applies high and forced-vacuum pressures for high-speed accelerated testing (10 Hz).

               · 300 MPa internal pressure loads can be applied     2. Multiple samples can be tested at the same time
                                                                                                                                                                                Mapping the Carbon
            Evaluating DLC Coating Stability                                                                                                      Mapping the Hardness of a Gear  Content of a Gear
            – Evaluating the Physical Properties of DLC Coating Layers by Microindentation Tests –

            Diamond-like carbon (DLC) coatings are thin, but very hard and can provide high wear resistance and high
            lubricity. Consequently, the coatings are often used on engine and fuel injection parts that involve significant
            sliding. DLC coatings are applied to target part surfaces by methods such as chemical vapor deposition
            (CVD) and sputtering. Though applying a DLC coating to flat surfaces is easy, forming the coating properly
            on bumpy surfaces can be difficult in some cases. The following is an example of microindentation tests
            using a DUH series ultra micro hardness tester as one means of evaluating whether or not reliable coating
            formation can be achieved on parts with complex shape.                   Dynamic Ultra Micro Hardness Testers
                                                                                            DUH-211 Series
              Description
                                                                                                                                                 Fully Automatic, from Measuring the Hardened Layer     Capable of Mapping the Content
                                                                         Test Force vs. Depth Graph
            The physical properties of DLC coatings applied with different coating conditions were   Test Force vs. Depth Graph
                                                                          40                                                                     Depth to Mapping Hardness Fully Automatic              of Carbon and Other Components
            compared. The results show the hardness and Young's modulus vary depending on the
            coating conditions.                                                                                                                    HMV-G31-FA Series Tester                               EPMA Series
                                                                                   No2          No1
            By performing tests with an indentation depth of about 1/10 the thickness of the coating
            layer, the physical properties of only the coating can be evaluated, without influence from
            the substrate material. Therefore, microindentation tests are perfect for DLC coatings only a   Test Force (mN)              · The edge detection function enables the sample shape to be automatically recognized and allows the testing position to
            few microns thick, which is commonly used in the automotive industry.
                                                                                                                                          be specified easily. This makes it possible to not only evaluate the depth of the hardened layer but also easily evaluate the
              Test Conditions                                                                                                             composition via hardness mapping.
              Test Mode:   Loading-unloading                                                                                             · The functional design provides a large and user-friendly work space, which is especially spacious in the depth direction and
                                                                          0
              Sample Name:  DLC coating (1 µm)                                          Depth (µm)        0.5                             there is an opening in the center area of the frame. That means the tester can directly test parts that were too big or long
              Test Load:   20 mN
              Loading Speed: 2.6 mN/sec                                                                                                   to test previously.
              Holding Time:  5 sec


               · Enables physical properties evaluation of only the coating layer.
               · Physical properties of DLC coating layers can be evaluated using a quick and simple method.




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