Page 3 - Shimadzu DSC-60 Plus Series
P. 3

High-sensitivity analysis across the entire measured
            temperature range



              High-Sensitivity Measurements of Trace Samples           Structure of the DSC-60 Plus Furnace



                   DSC
                   mW
                                                                   Newly designed the
                0.05                                               thermal resistance  Liquid nitrogen
                                                                   in these parts.
                           Sample Name:Sulfathiazole
                                0.005mg
                0.00
                                                                    Heater
                                                                                                    Heat transfer plate
                                             Peak Height
                                             −0.08mW
                -0.05
                                                                                                    Cooling fans
                                            173.9°C
                                                                           Thermo-uniformity
                -0.10
                                                                               plate
                          160.0      170.0       180.0
                                   Temp[°C]
                                                                Improved the temperature  Heat radiating fins
                                                                distribution around the
                                                                heater.
            A stable baseline and S/N performance enable the detection of   The new detector and new unique furnace construction
            a minute calorimetric change during trace analysis.  achieves a noise level of less than 0.5μW, ensuring a stable
                                                                baseline.

               Rubber and Plastic Materials
            In the analysis of rubbers and plastics, which are used in various industries, the DSC-60 Plus enables the detection of a complicated
            calorimetric change from low to high temperatures and the evaluation of the features of these materials.
                        DSC                                                 DSC
                        mW                                                  mW
                          Sample weight : 11.570[mg]                          Sample weight : 1.150[mg]
                      2.00
                                                                          1.00
                                                                                       176.3°C
                      1.00
                                                                                 145.0°C       −41.91J/g
                      0.00        −34.2°C                                 0.00
                      −1.00
                                                                         −1.00                  337.4°C
                      −2.00
                         −100.0  −50.0  0.0  50.0  100.0                        100.0  200.0  300.0  400.0
                                    Temp [°C]                                          Temp [°C]
                         Glass Transition of NBR Rubber                   Measurement of Engineering Plastic (PEEK)
               Battery and Electronic Parts
            The calorimetric measurement range has been extended three   the reactivity of chemical substances with comparatively large
            times (compared to previous Shimadzu instruments) to ±150   calorimetric change and for the measurement of the hardening
            mW. It offers an adequate dynamic range for the assessment of   reactions of adhesives.
                       DSC                                                   DSC
                       mW                                                    mW
                                                                         100.00
                        Sample weight : 6.730[mg]                             Sample weight : 45.450[mg]  135.0°C
                   10.00         231.2°C
                           213.8°C                                       80.00
                                     245.6°C
                                                                         60.00
                    5.00
                                        285.5°C
                                                                         40.00
                                                                                                189.15J/g
                    -0.00                                                20.00
                             200.0        300.0                                   50.0  100.0  150.0  200.0
                                  Temp [°C]                                             Temp[°C]
                 Measurement of Battery Material (LiB. Active material)        Adhesive Hardening Reaction
   1   2   3   4   5   6   7   8