Page 14 - Shimadzu AIM-9000

Automatic Automatic
Contaminant Qualitative
Recognition Analysis
Wide-Field High
Camera Finally, a wide view Sensitivity
on micro sample analysis
Application Examples in Specific Fields
Contaminant Micro
Analysis Surface Analysis
Analysis

Electrical and Electronic Pharmaceutical and Life

This is an analysis example of foreign matter attached to the terminal of an electronic part. By using a wide view camera, This is an analysis example of foreign substances adhering to the surface of a pharmaceutical tablet. By being taken to a
observing the entire part and deciding where to measure can be smoothly done. When a good spectrum is difficult to obtain diamond cell and rolled, transmission measurement can be performed to various shaped samples.
by reflection measurement, such as a thin stain or small alien substance, ATR spectroscopy (Ge prism) is effective.

Observation image of the Observation image of the
Observation image of the Observation image of the foreign tablet surface foreign matter on the
whole electronic part by matter on the terminal by 15× approximately 8 mm in diamond cell by 15×
the wide view camera Cassegrain objective mirror. diameter with the wide Cassegrain objective mirror.
view camera (2× zoom)
0.125
0.3
0.100
0.075 0.2
Abs Abs
0.050
0.1
0.025
0 0.0
4000 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 cm -1 4000 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 cm -1
Spectrum of the foreign matter acquired by reflection spectroscopy. It is estimated to be silicate. Identified as Silicate Spectrum of foreign matter collected in the diamond cell. Identified as Carbonate

Machinery and Transportation Petroleum and Chemical

This is a example of resin parts exposed to sunlight for a long period. This is the polarizing analysis of a film.
By measuring the infrared spectrum of the component cross section, the progress degree of the degradation about depth direction from By using the infrared polarizer, polarization property and orientation of the film can be evaluated.
the surface can be visualized.
CH2 twisting
1.5 0.08 vibration
Vertical Abs
Parallel H H 0.06 CH2 wagging
C C Vertical vibration
Deterioration H H n
Normal 0.04
1.0
Parallel
Abs 0.02
Abs
1250 1200 1150 1100 1050 1000 cm -1
0.5
3000 2000 1500 1000 cm -1 CH2 CH2 bending CH2 rocking
stretching vibration vibration

This sample had been exposed Imaging in the area 0.0
to the sunlight from the left side. of the C = O peak indicating oxidation degradation 3000 2000 1500 1000 cm -1

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